Cryogenic ultra-stable lasers have extremely low thermal noise limits and frequency drifts, but they are more seriously affected by vibration noise from cryostats. Main material candidates for cryogenic ultra-stable cavities include silicon and sapphire. Although sapphire has many excellent properties at low temperature, the development of sapphire-based cavities is less advanced than that of silicon-based. Using a homemade cryogenic sapphire cavity, we develop an ultra-stable laser source with a frequency instability of $1.9\times10^{-16}$. This is the best frequency instability level among similar systems using cryogenic sapphire cavities reported so far. Low vibration performance of the cryostat is demonstrated with a two-stage vibration isolation, and the vibration suppression is further improved by different mixing ratio of the gas-liquid helium. With this technique, vibrations at frequencies higher than tens of hertz are greatly suppressed.
To create a stable signal from a cryogenic sapphire maser frequency standard, the frequency-temperature dependence of the supporting Whispering Gallery mode must be annulled. We report the ability to control this dependence by manipulating the paramagnetic susceptibility of Fe3+ ions in the sapphire lattice. We show that the maser signal depends on other Whispering Gallery modes tuned to the pump signal near 31 GHz, and the annulment point can be controlled to exist between 5 to 10 K depending on the Fe3+ ion concentration and the frequency of the pump. This level of control has not been achie…
Here, we study the paramagnetic ions behavior in presence of a strong microwave electromagnetic field sustained inside a cryogenic sapphire whispering gallery mode resonator. The high frequency measurement resolution that can be now achieved by comparing two CSOs permit for the first time to observe clearly the non-linearity of the resonator power sensitivity. These observations that in turn allow us to optimize the CSO operation, are well explained by the Electron Spin Resonance (ESR) saturation of the paramagnetic impurities contained in the sapphire crystal.
We describe a liquid-cryogen free cryostat with ultra-low vibration levels which allows for continuous operation of a torsion balance at cryogenic temperatures. The apparatus uses a commercially available two-stage pulse-tube cooler and passive vibration isolation. The torsion balance exhibits torque noise levels lower than room temperature thermal noise by a factor of about four in the frequency range of 3-10mHz, limited by residual seismic motion and by radiative heating of the pendulum body. In addition to lowering thermal noise below room-temperature limits, the low-temperature environment…
We have applied laser calorimetry to the measurement of optical absorption in mono-crystalline sapphire at cryogenic temperatures. Sapphire is a promising candidate for the mirror substrates of the Large-scale Cryogenic Gravitational wave Telescope. The optical absorption coefficients of different sapphire samples at a wavelength of 1.064(micro)m at 5K were found to average 90ppm/cm.
The third-generation gravitational wave detectors are under development by operating the detector in cryogenic temperature to reduce the thermal noise. Silicon and sapphire are promising candidate materials for the test masses and suspension elements due to their remarkable mechanical and thermal properties at cryogenic temperature. Here we present the performances of the cryogenic thermal cycling and strength testing on hydroxide catalysis bonding between sapphire and silicon. Our results suggest that although these two materials have very different coefficients of thermal expansion, but if t…
We present the characterisation of three Cryogenic Sapphire Oscillators using the three-corner-hat method. Easily implemented with commercial components and instruments, this method reveals itself very useful to analyse the frequency stability limitations of these state-of-the-art ultra-stable oscillators. The best unit presents a fractional frequency stability better than 5e-16 at 1 s and below 2e-16 for integration times less than 5,000s.
We report the reduction of the thermal lensing in cryogenic sapphire mirrors, which is planed to be used in the Large scale Cryogenic Gravitational wave Telescope (LCGT) project. We measured three key parameters of sapphire substrate for thermal lensing at cryogenic temperature. They are optical absorption coefficient, thermal conductivity and temperature coefficient of refractive index at cryogenic temperature. On basis of these measurements, we estimated the shot noise sensitivity of the interferometer with thermal lensing by using a wave-front tracing simulation. We found that thermal lensi…
A large heat load caused by thermal radiation through a metal shield pipe was observed in a cooling test of a cryostat for a prototype of a cryogenic interferometric gravitational wave detector. The heat load was approximately 1000 times larger than the value calculated by the Stefan-Boltzmann law. We studied this phenomenon by simulation and experiment and found that it was caused by the conduction of thermal radiation in a metal shield pipe.
We report on the measurement and characterization of power to frequency conversion in the resonant mode of a cryogenic sapphire loaded cavity resonator, which is used as the frequency discriminating element of a loop oscillator circuit. Fluctuations of power incident on the resonator leads to changes in radiation pressure and temperature in the sapphire dielectric, both of which contribute to a shift in the resonance frequency. We measure a modulation and temperature independent radiation pressure induced power to frequency sensitivity of -0.15 Hz/mW and find that this is the primary factor li…
The Cryogenic Sapphire Oscillator is today recognized for its unprecedented frequency stability, mainly coming from the exceptional physical properties of its resonator made in a high quality sapphire crystal. With these instruments, the fractional frequency measurement resolution, currently of the order of 1e-16, is such that it is possible to detect very small phenomena like residual resonator environmental sensitivities. Thus, we highlighted an unexpected magnetic sensitivity of the Cryogenic Sapphire Oscillator (CSO) at low magnetic field. The fractional frequency sensitivity has been prel…
We developed an apparatus to couple a 50-micrometer diameter whispering-gallery silica microtoroidal resonator in a helium-4 cryostat using a straight optical tapered-fiber at 1550nm wavelength. On a top-loading probe specifically adapted for increased mechanical stability, we use a specifically-developed "cryotaper" to optically probe the cavity, allowing thus to record the calibrated mechanical spectrum of the optomechanical system at low temperatures. We then demonstrate excellent thermalization of a 63-MHz mechanical mode of a toroidal resonator down to the cryostat's base temperature of 1…
A system providing an optical frequency with an instability comparable to that of a hydrogen maser is presented. It consists of a $5$ $\mathrm{cm}$ long, vertically oriented silicon optical resonator operated at temperatures between $1.5$ $\mathrm{K}$ and $3.6$ $\mathrm{K}$ in a closed-cycle cryostat with low-temperature Joule-Thomson stage. We show that with a standard cryostat, a simple cryogenic optomechanical setup, no active or passive vibration isolation, a minimum frequency instability of $2.5\times10^{-15}$ at $τ=1500$ $\mathrm{s}$ integration time can be reached. The influence of puls…
We report on the evaluation of microwave frequency synthesis using two cryogenic sapphire oscillators developed at the University of Western Australia. A down converter is used to make comparisons between microwave clocks at different frequencies, where the synthesized signal has a stability not significantly different from the reference oscillator. By combining the CSO with a H-maser, a reference source of arbitrary frequency at X-band can be synthesized with a fractional frequency stability of sub-$4 \times 10^{-15}$ for integration times between 1 s and 10,000 s.
KAGRA uses cryogenics to cool its sapphire test masses down to 20 K to reduce the thermal noise. However, cryocooler vibration and structural resonances of the cryostat couple to test mass and can contaminate the detector sensitivity. We performed vibration analysis of the cooling system at cryogenic temperature to study its impact on detector sensitivity. Our measurement show shield vibration below 1 Hz is not impacted by cryocooler operation or structural resonances and follows ground motion. The noise floor of the shield in 1-100 Hz was observed to be 2-3 order of magnitude larger than seis…
A Cryogenic Sapphire Oscillator has been implemented at 11.2 GHz using a low-vibration design pulse-tube cryocooler. Compared with a state-of-the-art liquid helium cooled CSO in the same laboratory, the square root Allan variance of their combined fractional frequency instability is $σ_y = 1.4 \times 10^{-15}τ^{-1/2}$ for integration times $1 < τ< 10$ s, dominated by white frequency noise. The minimum $σ_y = 5.3 \times 10^{-16}$ for the two oscillators was reached at $τ= 20$ s. Assuming equal contributions from both CSOs, the single oscillator phase noise $S_ϕ \approx -96 \; dB \; rad^2/Hz$ at…
We report on the development of a sapphire cryogenic microwave resonator oscillator long-term fractional frequency stability of 2x10^-17Sqrt[τ] for integration times τ>10^3 s and negative drift of about 2.2x10^-15/day. The short-term frequency instability of the oscillator is highly reproducible and also state-of-the-art: 5.6x10^-16 for an integration time of τ~ 20 s.
In this work we present an elegant solution for a scintillation counter to be integrated into a cryogenic system. Its distinguishing feature is the absence of a continuous light guide coupling the scintillation and the photodetector parts, operating at cryogenic and room temperatures respectively. The prototype detector consists of a plastic scintillator with glued-in wavelength-shifting fiber located inside a cryostat, a Geiger-mode Avalanche Photodiode (G-APD) outside the cryostat, and a lens system guiding the scintillation light re-emitted by the fiber to the G-APD through optical windows …
The cryogenic sapphire oscillator (CSO) is a highly specialized machine, which delivers a reference signal exhibiting the lowest frequency fluctuations. For the best units, the Allan deviation (ADEV) is <1e-15 for integration time between 1 and 10,000 s, with a drift <1e-14 in one day.The oscillator is based on a sapphire monocrystal resonating at 10 GHz in a whispering-gallery mode, cooled at 6 K for highest Q-factor and zero thermal coefficient. We report on the progress accomplished implementing eleven CSOs in about 10 years since the first sample delivered to the ESA station in Argentina. …
We present two simple cryogenic RF ion trap systems in which cryogenic temperatures and ultra high vacuum pressures can be reached in as little as 12 hours. The ion traps are operated either in a liquid helium bath cryostat or in a low vibration closed cycle cryostat. The fast turn around time and availability of buffer gas cooling made the systems ideal for testing surface-electrode ion traps. The vibration amplitude of the closed cycled cryostat was found to be below 106 nm. We evaluated the systems by loading surface-electrode ion traps with $^{88}$Sr$^+$ ions using laser ablation, which is…
A low maintenance long-term operational cryogenic sapphire oscillator has been implemented at 11.2 GHz using an ultra-low-vibration cryostat and pulse-tube cryocooler. It is currently the world's most stable microwave oscillator employing a cryocooler. Its performance is explained in terms of temperature and frequency stability. The phase noise and the Allan deviation of frequency fluctuations have been evaluated by comparing it to an ultra-stable liquid-helium cooled cryogenic sapphire oscillator in the same laboratory. Assuming both contribute equally, the Allan deviation evaluated for the c…
Open-access microcavities are a powerful tool to enhance light-matter interactions for solid-state quantum and nano systems and are key to advance applications in quantum technologies. For this purpose, the cavities should simultaneously meet two conflicting requirements - full tunability to cope with spatial and spectral inhomogeneities of a material, and highest stability under operation in a cryogenic environment to maintain resonance conditions. To tackle this challenge, we have developed a fully-tunable, open-access, fiber-based Fabry-Pérot microcavity platform which can be operated also …
Construction of a large-scale cryogenic gravitational-wave telescope KAGRA has been completed and the four sapphire test masses have been installed in cryostat vacuum chambers. It recently turned out that a sapphire substrate used for one of the input test masses shows a characteristic strcuture in its transmission map due to non-uniformity of the crystal. We performed an interferometer simulation to see the influence of the non-uniformity using measured transmission/reflection maps.
This article shows the first measurement of three 100 MHz signals exhibiting fluctuations from 2E-16 to parts in 1E-15 for integration time tau between 1 s and 1 day. Such stable signals are provided by three Cryogenic Sapphire Oscillators (CSOs) operating at about 10 GHz, also delivering the 100 MHz output via a dedicated synthesizer. The measurement is made possible by a 6-channel Tracking DDS (TDDS) and the two-sample covariance tool, used to estimate the Allan variance. The use of two TDDS channels per CSO enables high rejection of the instrument background noise. The covariance outperform…
The cryogenic underground observatory for rare events (CUORE) is a 1-ton scale bolometric experiment whose detector consists of an array of 988 TeO2 crystals arranged in a cylindrical compact structure of 19 towers. This will be the largest bolometric mass ever operated. The experiment will work at a temperature around or below 10 mK. CUORE cryostat consists of a cryogen-free system based on pulse tubes and a custom high power dilution refrigerator, designed to match these specifications. The cryostat has been commissioned in 2014 at the Gran Sasso National Laboratories and reached a record te…
Detectors in particle physics, particularly when including cryogenic components, are often enclosed in vessels that do not provide any physical or visual access to the detectors themselves after installation. However, it can be desirable for experiments to visually investigate the inside of the vessel. The MicroBooNE cryostat hosts a TPC with sense-wire planes, which had to be inspected for damage such as breakage or sagging. This paper describes an approach to view the inside of the MicroBooNE cryostat with a setup of a camera and a mirror through one of its cryogenic service nozzles. The pap…
We present new results from our test of Lorentz invariance, which compares two orthogonal cryogenic sapphire microwave oscillators rotating in the lab. We have now acquired over 1 year of data, allowing us to avoid the short data set approximation (less than 1 year) that assumes no cancelation occurs between the $\tildeκ_{e-}$ and $\tildeκ_{o+}$ parameters from the photon sector of the standard model extension. Thus, we are able to place independent limits on all eight $\tildeκ_{e-}$ and $\tildeκ_{o+}$ parameters. Our results represents up to a factor of 10 improvement over previous non rotati…
The Horizontal Test Stand (HTS) SRF Cavity and Cryomodule 1 (CM1) of eight 9-cell, 1.3GHz SRF cavities are operating at Fermilab. For the cryogenic control system, how to hold liquid level constant in the cryostat by regulation of its Joule-Thompson JT-valve is very important after cryostat cool down to 2.0 K. The 72-cell cryostat liquid level response generally takes a long time delay after regulating its JT-valve; therefore, typical PID control loop should result in some cryostat parameter oscillations. This paper presents a type of PID parameter self-optimal and Time-Delay control method us…
The Cryogenic Underground Observatory for Rare Events (CUORE) is a bolometric experiment for neutrinoless double-beta decay in $^{130}$Te search, currently taking data at the underground facility of Laboratori Nazionali del Gran Sasso (LNGS). The CUORE cryostat successfully cooled down a mass of about 1 ton at $\sim$7\,mK, delivering an uniform and constant base temperature. This result marks a fundamental milestone in low temperature detectors techniques, opening the path for future ton-scale bolometric experiments searching for rare events. In this paper we present the CUORE cryogenic infras…
We present here a small-scale liquid Helium (LHe) immersion cryostat with an innovative optical setup suitable to work in long wavelength radiation ranges and under applied magnetic field. The cryostat is a multi stage device with several shielding in addition to several optical stages. The system has been designed with an external liquid Nitrogen boiler to reduce the liquid bubbling. The optical and mechanical properties of the optical elements were calculated and optimized for the designed configuration while the optical layout has been simulated and optimized among different configurations …
Detectors for direct dark matter search using noble gases in liquid phase as detection medium need to be coupled to liquefaction, purification and recirculation systems. A dedicated cryogenic system has been assembled and operated at the INFN-Naples cryogenic laboratory with the aim to liquefy and purify the argon used as active target in liquid argon detectors to study the scintillation and ionization signals detected by large SiPMs arrays. The cryogenic system is mainly composed of a double wall cryostat hosting the detector, a purification stage to reduce the impurities below one part per b…
Cryogenic Sapphire Oscillators (CSO) developed at UWA have now been in operation around the world continuously for many years. Such oscillators, due to their excellent spectral purity are essential for interrogating atomic frequency standards at the limit of quantum projection noise; otherwise aliasing effects will dominate the frequency stability due to the periodic sampling between successive interrogations of the atomic transition. For this reason, UWA oscillators are now operational at NMI (Sydney), LNE-SYRTE (Paris), the French Space Agency (CNES, Toulouse) and at UWA (Perth). Other appli…
Two nominally identical ultra-stable cryogenic microwave oscillators are compared. Each incorporates a dielectric-sapphire resonator cooled to near 6 K in an ultra-low vibration cryostat using a low-vibration pulse-tube cryocooler. The phase noise for a single oscillator is measured at -105 dBc/Hz at 1 Hz offset on the 11.2 GHz carrier. The oscillator fractional frequency stability is characterized in terms of Allan deviation by 5.3 x 10^-16 tau^-1/2 + 9 x 10^-17 for integration times 0.1 s < tau < 1000 s and is limited by a flicker frequency noise floor below 1 x 10^-16. This result is better…
The phase noise and frequency stability measurements of 1 GHz, 100 MHz, and 10 MHz signals are presented which have been synthesized from microwave cryogenic sapphire oscillators using ultra-low-vibration pulse-tube cryocooler technology. We present the measured data using independent cryogenic oscillators for the 100 MHz and 10 MHz synthesized signals, whereas previously we only estimated the expected results based on residual phase noise measurements, when only one cryogenic oscillator was available. In addition we present the design of a 1 GHz synthesizer using a Crystek voltage controlled …
We present the characterization of 8-12 GHz whispering gallery mode resonators machined in high-quality sapphire crystals elaborated with different growth techniques. These microwave resonators are intended to constitute the reference frequency of ultra-stable Cryogenic Sapphire Oscillators. We conducted systematic tests near 4 K on these crystals to determine the unloaded Q-factor and the turnover temperature for whispering gallery modes in the 8-12 GHz frequency range. These characterizations show that high quality sapphire crystals elaborated with the Heat Exchange or the Kyropoulos growth …
We present the design and first measurement results for an ultra-stable cryogenically cooled optical sapphire resonator system with a potential relative frequency stability better than 3x10^-17. This level of oscillator stability allows for more precise tests of Einstein's theories of relativity and thus could help to find first hints of "new physics". We will give some details on a projected experiment to test Lorentz invariance that will utilize these cavities.
High-finesse, open-geometry microcavities have recently emerged as a versatile tool for enhancing interactions between photons and material systems, with a range of applications in quantum optics and quantum information science. However, mechanical vibrations pose a considerable challenge to their operation within a closed-cycle cryostat, particularly when spatial tunability and free-space optical access are required. Here, we present the design and characterization of a system that can achieve $\sim$16 pm-rms passive mechanical stability between two high-finesse mirrors while permitting both …
Cryogenic quantum sensing techniques are developing alongside the ever-increasing requirements for noiseless experimental environments. For instance, several groups have isolated internal system vibrations from cold heads in closed-cycle dilution refrigerators. However, these solutions often do not account for external vibrations, necessitating novel strategies to isolate the entire cryogenic systems from their environments in a particular set of raised cryostats. Here, we introduce a dual-stage external active vibration-isolation solution in conjunction with a closed-cycle dilution refrigerat…
We describe the cryogenic system for SPIDER, a balloon-borne microwave polarimeter that will map 8% of the sky with degree-scale angular resolution. The system consists of a 1284 L liquid helium cryostat and a 16 L capillary-filled superfluid helium tank, which provide base operating temperatures of 4 K and 1.5 K, respectively. Closed-cycle helium-3 adsorption refrigerators supply sub-Kelvin cooling power to multiple focal planes, which are housed in monochromatic telescope inserts. The main helium tank is suspended inside the vacuum vessel with thermally insulating fiberglass flexures, and sh…
Monitoring motion originating from ultra low-temperature cooling systems like cryocoolers is important for vibration sensitive cryogenic experiments like KAGRA. Since no commercial cryogenic accelerometers are available, we developed a compact self-calibrating accelerometer with a Michelson interferometer readout for cryogenic use. Change in calibration factor and drop in interferometer output originating from temperature drop were the main concerns which were tackled. Sensitivity of $3.38\times10^{-11}$ m/$\sqrt{\mathrm{Hz}}$ at 1 Hz was achieved at 300 K. The accelerometer was tested inside …
Pulse-tube based dilution refrigerators are massively employed in low temperature physics. They allow to reduce the running costs and to be operated with unprecedented easiness. However, the main drawback of this technology is the mechanical vibrations induced by the pulse-tube cryocooler. These perturbations can cause extra-noises drastically affecting the detector performance. In this paper, we propose a solution to mitigate the impact of these vibrations by mounting the detectors in an elastic-pendulum based suspended tower. Based on vibration modeling and experimental tests, we show that t…
Liquid Helium is used widely, from hospitals to characterization of materials at low temperatures. Many experiments at low temperatures require liquid Helium, particularly when vibration isolation precludes the use of cryocoolers and when one needs to cool heavy equipment such as superconducting coils. Here we describe methods to simplify the operations required to use liquid Helium by eliminating the use of high pressure bottles, avoiding blockage and improving heating and cooling rates. First we show a simple and very low cost method to transfer liquid Helium from a transport container into …
The introduction of an optical resonator can enable efficient and precise interaction between a photon and a solid-state emitter. It facilitates the study of strong light-matter interaction, polaritonic physics and presents a powerful interface for quantum communication and computing. A pivotal aspect in the progress of light-matter interaction with solid-state systems is the challenge of combining the requirements of cryogenic temperature and high mechanical stability against vibrations while maintaining sufficient degrees of freedom for in-situ tunability. Here, we present a fiber-based open…
We describe the design and in--flight performance of the cryostat and the self-contained $^{3}$He refrigerator for the OLIMPO balloon--borne experiment, a spectrophotometer to measure the Sunyaev-Zel'dovich effect in clusters of galaxies. The $^{3}$He refrigerator provides the 0.3 K operation temperature for the four arrays of kinetic inductance detectors working in 4 bands centered at 150, 250, 350 and 460 GHz. The cryostat provides the 1.65 K base temperature for the $^{3}$He refrigerator, and cools down the reimaging optics and the filters chain at about 2 K. The integrated system was desig…
We present a Michelson-Morley type experiment for testing the isotropy of the speed of light in vacuum and matter. The experiment compares the resonance frequency of an actively rotated monolithic optical cryogenic sapphire resonator against the resonance frequency of a stationary evacuated optical cavity made of ultra-low-expansion glass. The results yield an upper limit for the anisotropy of the speed of light in matter (sapphire) of Delta(c)/c < 1 x 10^-16, limited by the frequency stability of the sapphire resonator.
We have developed low temperature part of an ultra high vacuum scanning probe microscope (UHV-SPM) working at variable temperature within the range from 20 K to 700 K. To achieve the required temperature range, a flow cooling system using cryogenic helium (~5 K) as a coolant was designed. The system consists of a flow cryostat and a flexible low-loss transfer line connecting a Dewar vessel with the flow cryostat. We have also tested liquid nitrogen (~ 77 K) as an alternative low-cost coolant. Using nitrogen, the microscope can operate at temperatures of about 100 K and higher. As the flow of t…
Amplification is usually necessary when measuring the frequency instability of microwave signals. In this work, we develop a flicker noise free frequency measurement system based on a common or shared amplifier. First, we show that correlated flicker phase noise can be cancelled in such a system. Then we compare the new system with the conventional by simultaneously measuring the beat frequency from two cryogenic sapphire oscillators with parts in 10^15 fractional frequency instability. We determine for low power, below -80 dBm, the measurements were not limited by correlated noise processes b…
