PandaX-4T, the new generation of the PandaX detector, is a xenon dual-phase detector with about six tons of liquid xenon as target for dark matter search. A cryogenics and xenon handling system is designed to liquify and purify this large detector. In this paper, the results on the commission of the cryogenics and gas handling system are reported. The maximum cooling power of ~ 580 W at 178 K with three cooperating coldheads has been achieved. The filling rate with an assisted liquid nitrogen cooling can reach ~ 700 kg/day. The average rate of recuperation by liquid nitrogen is around 440 kg/day. The maximum total purification speed of two circulation loops is up to ~ 155 slpm. Each loop is using a large heat exchanger with a measured heat exchange efficiency of ~ 97.5+-0.5%.
This paper describes results on R&D of an economical and efficient cryogenic system prototype for future liquid xenon detector. The test module of the prototype has a "cold head" attached to a copper rod, which is specially designed to transport heat loads to a free-boiling liquid nitrogen bath. The performance of the test module and commercial refrigerators is compared. The module with an optimized copper rod has demonstrated more than 1500W cooling power at 178K.The temperature of the "cold head" can be kept stable with an error of 0.02K, its fluctuation is within 0.1K.
An efficient cryogenic distillation system was designed and constructed for PandaX-4T dark matter detector based on the McCabe-Thiele (M-T) method and the conservation of mass and energy. This distillation system is designed to reduce the concentration of krypton in commercial xenon from 5X$10^{-7}$ mol/mol to $10^{-14}$ mol/mol with 99% xenon collection efficiency at a maximum flow rate of 10 kg/h. The offline distillation operation has been completed and 5.75 tons of ultra-high purity xenon was produced, which is used as the detection medium in PandaX-4T detector. The krypton concentration o…
Design, construction, and testing of the PandaX-xT cryogenics system
Shanghai Jiao Tong University（上海交通大学）；Shanghai Jiao Tong University Sichuan Research Institute（上海交通大学四川研究院）；Sun Yat-Sen University（中山大学）；Yalong River Hydropower Development Company, Ltd.（雅砻江流域水电开发有限公司）
In order to recuperate the ultra-high purity xenon from PandaX-4T dark matter detector to high-pressure gas cylinders in emergency or at the end-of-run situation, a high speed ultra-high purity xenon recuperation system is designed and developed. This system includes a diaphragm pump, the heat management system, the main recuperation pipeline, the reflux pipeline, the auxiliary recuperation pipeline and the automatic control system. The liquid xenon in the detector is vaporized by the heat management system, and the gaseous xenon is compressed to 6 MPa at the flow rate of 200 standard litres p…
An online cryogenic distillation system for the removal of krypton and radon from xenon was designed and constructed for PandaX-4T, a highly sensitive dark matter detection experiment. The krypton content in a commercial xenon product is expected to be reduced by 7 orders of magnitude with 99% xenon collection efficiency at a flow rate of 10 kg/h by design. The same system can reduce radon content in xenon by reversed operation, with an expected radon reduction factor of about 1.8 in PandaX-4T under a flow rate of 56.5 kg/h. The commissioning of this system was completed, with krypton and rado…
We report the long term performance of the photosensors, 143 one-inch R8520-406 and 37 three-inch R11410-MOD photomultipliers from Hamamatsu, in the first phase of the PandaX dual-phase xenon dark matter experiment. This is the first time that a significant number of R11410 photomultiplier tubes were operated in liquid xenon for an extended period, providing important guidance to the future large xenon-based dark matter experiments.
We report the Neutrino-less Double Beta Decay (NLDBD) search results from PandaX-II dual-phase liquid xenon time projection chamber. The total live time used in this analysis is 403.1 days from June 2016 to August 2018. With NLDBD-optimized event selection criteria, we obtain a fiducial mass of 219 kg of natural xenon. The accumulated xenon exposure is 242 kg$\cdot$yr, or equivalently 22.2 kg$\cdot$yr of $^{136}$Xe exposure. At the region around $^{136}$Xe decay Q-value of 2458 keV, the energy resolution of PandaX-II is 4.2%. We find no evidence of NLDBD in PandaX-II and establish a lower limi…
The dual-phase xenon time projection chamber (TPC) is one of the most sensitive detector technology for dark matter direct search, where the energy deposition of incoming particle can be converted into photons and electrons through xenon excitation and ionization. The detector response to signal energy deposition varies significantly with the electric field in liquid xenon. We study the detector's light yield and its dependence on the electric field in the PandaX-II dual-phase detector containing 580~kg liquid xenon in the sensitive volume. From our measurements, the light yield at electric fi…
PandaX-II experiment is a dark matter direct detection experiment using about half-ton of liquid xenon as the sensitive target. The electrical pulses detected by photomultiplier tubes from scintillation photons of xenon are recorded by waveform digitizers. The data acquisition of Pandax-II relies on a trigger system that generates common trigger signals for all waveform digitizers. Previously an analog device-based trigger system was used for the data acquisition system. In this paper we present a new FPGA-based trigger system. The design of this system and trigger algorithms are described. Th…
PandaX-4T is a dark matter direct detection experiment located in China jinping underground laboratory. The central apparatus is a dual-phase xenon detector containing 4 ton liquid xenon in the sensitive volume, with about 500 photomultipliers instrumented in the top and the bottom of the detector. In this paper we present a completely new system of readout electronics and data acquisition in the PandaX-4T experiment. Compared to the one used in the previous PandaX dark matter experiments, the new system features triggerless readout and higher bandwidth. With triggerless readout, dark matter s…
At the China Jinping Underground Laboratory, the Particle AND Astrophysical Xenon phase IV (PandaX-4ton) in planning is a dark matter direct detection experiment with dual-phase xenon detector as an upgrade of the second phase of the experiment, PandaX-II. In this paper, the prototype of the front-end electronics of PandaX-4ton is presented. The front-end electronics consist of the high-gain preamplifier cards and the eight-channel digitizers with 14-bit resolution and 1 GSps sampling rate for waveform digitization. The clock synchronization circuit within the digitizer is well-designed to ali…
We report a systematic determination of the responses of PandaX-II, a dual phase xenon time projection chamber detector, to low energy recoils. The electron recoil (ER) and nuclear recoil (NR) responses are calibrated, respectively, with injected tritiated methane or $^{220}$Rn source, and with $^{241}$Am-Be neutron source, within an energy range from $1-25$ keV (ER) and $4-80$ keV (NR), under the two drift fields of 400 and 317 V/cm. An empirical model is used to fit the light yield and charge yield for both types of recoils. The best fit models can well describe the calibration data. The sys…
The purpose of the PandaX experiments is to search for the possible events resulted from dark matter particles, neutrinoless double beta decay or other rare processes with xenon detectors. Understanding the energy depositions from backgrounds or calibration sources in these detectors is very important. The program of BambooMC is created to perform the Geant4-based Monte Carlo simulation, providing reference information for the experiments. We introduce the design and features of BambooMC in this report. The running of the program depends on a configuration file, which combines different detect…
We discuss an in-situ evaluation of the $^{85}$Kr, $^{222}$Rn, and $^{220}$Rn background in PandaX-I, a 120-kg liquid xenon dark matter direct detection experiment. Combining with a simulation, their contributions to the low energy electron-recoil background in the dark matter search region are obtained.
The PandaX project consists of a series of xenon-based experiments that are used to search for dark matter (DM) particles and to study the fundamental properties of neutrinos. The next DM experiment PandaX-4T will be using 4 ton liquid xenon in the sensitive volume, which is nearly a factor of seven larger than that of the previous experiment PandaX-II. Due to the increasing target mass, the sensitivity of searching for both DM and neutrinoless double-beta decay ($0νββ$) signals in the same detector will be significantly improved. However, the typical energy of interest for $0νββ$ signals is a…
PandaX is a large upgradable liquid-xenon detector system that can be used for both direct dark-matter detection and $^{136}$Xe double-beta decay search. It is located in the Jinping Deep-Underground Laboratory in Sichuan, China. The detector operates in dual-phase mode, allowing detection of both prompt scintillation, and ionization charge through proportional scintillation. The central time projection chamber will be staged, with the first stage accommodating a target mass of about 120\,kg. In stage II, the target mass will be increased to about 0.5\,ton. In the final stage, the detector can…
We describe the electronics and data acquisition system used in the first phase of the PandaX experiment -- a 120 kg dual-phase liquid xenon dark matter direct detection experiment in the China Jin-Ping Underground Laboratory. This system utilized 180 channels of commercial flash ADC waveform digitizers. This system achieved low trigger threshold ($<$1 keV electron-equivalent energy) and low deadtime data acquistion during the entire experimental run.
The two-phase xenon detector is at the frontier of dark matter direct search. This kind of detector uses liquid xenon as the sensitive target and is operated in two-phase (liquid/gas) mode, where the liquid level needs to be monitored and controlled in sub-millimeter precision. In this paper, we present a detailed design and study of two kinds of level meters for the PandaX dark matter detector. The long level meter is used to monitor the overall liquid level while short level meters are used to monitor the inclination of the detector. These level meters are cylindrical capacitors custom-made …
We discuss recent advances in the development of cryogenic gaseous photomultipliers (GPM), for possible use in dark matter and other rare-event searches using noble-liquid targets. We present results from a 10 cm diameter GPM coupled to a dual-phase liquid xenon (LXe) TPC, demonstrating - for the first time - the feasibility of recording both primary ("S1") and secondary ("S2") scintillation signals. The detector comprised a triple Thick Gas Electron Multiplier (THGEM) structure with cesium iodide photocathode on the first element; it was shown to operate stably at 180 K with gains above 10^5,…
The PandaX-III experiment uses a high pressure xenon gas TPC to search for the NLDBD of $^{136}$Xe. The Microbulk Micromegas will be used for charge amplification and readout in order to record both the energy and track of an event with high energy resolution and spatial resolution. In the first phase of the experiment, we are building a detector which contains 140 kg 90\% $^{136}$Xe enriched gas operated at 10 bar. The detector will be installed in a dry shielding system at CJPL-II. In this paper, we wil report the design of the PandaX-III detector, including the shielding of the experiment a…
Two cryogenic bath-type heat exchangers for ultra-pure noble gas applications were developed with particular emphasis on noble gas liquefaction in cryogenic distillation systems. The main objective was to construct heat exchangers for xenon from materials that do not emanate radon and that fulfill ultra-high vacuum standards. Therefore, only high-quality copper and stainless steel materials were used. Especially, large-area oxygen-free copper fins with high conductivity in a new design ensure efficient heat transfer. One bath-type Xe-Xe heat exchanger was designed with a diameter of 50 cm to a…
We report on the custom produced low radiation background stainless steel and the welding rod for the PandaX experiment, one of the deep underground experiments to search for dark matter and neutrinoless double beta decay using xenon. The anthropogenic 60 Co concentration in these samples is at the range of 1 mBq/kg or lower. We also discuss the radioactivity of nuclear-grade stainless steel from TISCO which has a similar background rate. The PandaX-II pressure vessel was thus fabricated using the stainless steel from CISRI and TISCO. Based on the analysis of the radioactivity data, we also ma…
We have developed an efficient cryogenic system with heat exchange and associated gas purification system, as a prototype for the XENON1T experiment. The XENON1T detector will use about 3 ton of liquid xenon (LXe) at a temperature of 175K as target and detection medium for a dark matter search. In this paper we report results on the cryogenic system performance focusing on the dynamics of the gas circulation-purification through a heated getter, at flow rates above 50 Standard Liter per Minute (SLPM). A maximum flow of 114 SLPM has been achieved, and using two heat exchangers in parallel, a he…
The Particle And Astrophysical Xenon Experiment III (PandaX-III) is an experiment to search for the Neutrinoless Double Beta Decay (NLDBD) using 200 kg radio-pure high-pressure gaseous xenon TPC with Micromegas detectors at both ends and cathode in the middle. A small-scale TPC equipped with 7 Microbulk Micromegas detectors is developed as the prototype detector. 128 channels are readout following an X-Y design with strips of 3 mm pitch (64 channels each direction) from one Micromegas module. Highly integrated front-end electronics composed of 4 front-end cards with 1024 readout channels is de…
The PandaX-II experiment employed a 580kg liquid xenon detector to search for the interactions between dark matter particles and the target xenon atoms. The accidental coincidences of isolated signals result in a dangerous background which mimic the signature of the dark matter. We performed a detailed study on the accidental coincidence background in PandaX-II, including the possible origin of the isolated signals, the background level and corresponding background suppression method. With a boosted-decision-tree algorithm, the accidental coincidence background is reduced by 70% in the dark ma…
The PandaX-III (Particle And Astrophysical Xenon Experiment III) experiment will search for Neutrinoless Double Beta Decay (NLDBD) of 136Xe at the China Jin-Ping underground Laboratory II (CJPL-II). In the first phase of the experiment, a high pressure gas Time Projection Chamber (TPC) will contain 200 kg, 90% 136Xe enriched gas operated at 10 bar. Microbulk Micromegas, a fine pitch micro-pattern gas detector, will be used for charge readout and enable us to reconstruct tracks of NLDBD events with good energy and spatial resolution. With simulation, we demonstrate excellent background suppress…
The search for the neutrinoless double beta decay (0$νββ$) is one of the most important quests nowadays in neutrino physics. Among the different techniques used, high pressure xenon (HPXe) gas time projection chambers (TPC) stand out because they allow to image the topology of the 0$νββ$ event (one straggling track ending in two blobs), and use it to discriminate signal from background events. Recent results with microbulk Micromegas in Xe + trimethylamine (TMA) mixtures show high promise in terms of gain, stability of operation, and energy resolution at high pressures (up to 10 bar). The addi…
The Hamamatsu R11410 photomultiplier, a tube of 3" diameter and with a very low intrinsic radioactivity, is an interesting light sensor candidate for future experiments using liquid xenon (LXe) as target for direct dark matter searches. We have performed several experiments with the R11410 with the goal of testing its performance in environments similar to a dark matter detector setup. In particular, we examined its long-term behavior and stability in LXe and its response in various electric field configurations.
Neutron-induced nuclear recoil background is critical to the dark matter searches in the PandaX-4T liquid xenon experiment. This paper studies the feature of neutron background in liquid xenon and evaluates their contribution in the single scattering nuclear recoil events through three methods. The first method is fully Monte Carlo simulation based. The last two are data-driven methods that also use the multiple scattering signals and high energy signals in the data, respectively. In the PandaX-4T commissioning data with an exposure of 0.63 tonne-year, all these methods give a consistent resul…
We report the results of a weakly-interacting massive particle (WIMP) dark matter search using the full 80.1\;live-day exposure of the first stage of the PandaX experiment (PandaX-I) located in the China Jin-Ping Underground Laboratory. The PandaX-I detector has been optimized for detecting low-mass WIMPs, achieving a photon detection efficiency of 9.6\%. With a fiducial liquid xenon target mass of 54.0\,kg, no significant excess event were found above the expected background. A profile likelihood analysis confirms our earlier finding that the PandaX-I data disfavor all positive low-mass WIMP …
The XENON1T experiment aims for the direct detection of dark matter in a cryostat filled with 3.3 tons of liquid xenon. In order to achieve the desired sensitivity, the background induced by radioactive decays inside the detector has to be sufficiently low. One major contributor is the $β$-emitter $^{85}$Kr which is an intrinsic contamination of the xenon. For the XENON1T experiment a concentration of natural krypton in xenon $\rm{^{nat}}$Kr/Xe < 200 ppq (parts per quadrillion, 1 ppq = 10$^{-15}$ mol/mol) is required. In this work, the design of a novel cryogenic distillation column using the …
Results of WIMP dark matter search from the first data of the PandaX-II experiment are presented. PandaX-II experiment uses a 500 kg scale dual phase liquid xenon time projection chamber, operating at the China JinPing Underground Laboratory. The first data correspond to a total exposure of $3.1\times10^{4}$ kg-day. The observed data after selections are found to be consistent with background expection, and upper limits of the spin-independent WIMP-nucleon cross sections are derived for a range of WIMP mass between 5 GeV/c$^2$ and 1000 GeV/$c^{2}$. The lowest cross section limit obtained is 2.…
XeBRA is a flexible cryogenic platform designed to perform research and development for liquid xenon detectors searching for rare events. Its extra-large outer cryostat makes it possible to install a wide variety of detector designs. We present the system, including its cryogenic, gas handling, data acquisition and slow control subsystems. Two dual phase time projection chambers with sensitive masses at the 1 kg scale have so far been operated in XeBRA. Using data from these, we determine the field-dependence of the electron drift velocity in liquid xenon. We also measure the relative charge a…
We report on the first dark-matter (DM) search results from PandaX-I, a low threshold dual-phase xenon experiment operating at the China Jinping Underground Laboratory. In the 37-kg liquid xenon target with 17.4 live-days of exposure, no DM particle candidate event was found. This result sets a stringent limit for low-mass DM particles and disfavors the interpretation of previously-reported positive experimental results. The minimum upper limit, $3.7\times10^{-44}$\,cm$^2$, for the spin-independent isoscalar DM-particle-nucleon scattering cross section is obtained at a DM-particle mass of 49\,…
We have developed a low-energy electron recoil (ER) calibration method with $^{220}$Rn for the PandaX-II detector. $^{220}$Rn, emanated from natural thorium compounds, was fed into the detector through the xenon purification system. From 2017 to 2019, we performed three dedicated calibration campaigns with different radon sources. We studied the detector response to $α$, $β$, and $γ$ particles with focus on low energy ER events. During the runs in 2017 and 2018, the amount of radioactivity of $^{222}$Rn were on the order of 1\% of that of $^{220}$Rn and thorium particulate contamination was ne…
We describe the purification of xenon from traces of the radioactive noble gas radon using a cryogenic distillation column. The distillation column is integrated into the gas purification loop of the XENON100 detector for online radon removal. This enabled us to significantly reduce the constant $^{222}$Rn background originating from radon emanation. After inserting an auxiliary $^{222}$Rn emanation source in the gas loop, we determined a radon reduction factor of R > 27 (95% C.L.) for the distillation column by monitoring the $^{222}$Rn activity concentration inside the XENON100 detector.
We present the performances and characterization of an array made of S13370-3050CN (VUV4 generation) Multi-Pixel Photon Counters manufactured by Hamamatsu and equipped with a low power consumption preamplifier operating at liquid xenon temperature (~ 175 K). The electronics is designed for the readout of a matrix of maximum dimension of 8 x 8 individual photosensors and it is based on a single operational amplifier. The detector prototype presented in this paper utilizes the Analog Devices AD8011 current feedback operational amplifier, but other models can be used depending on the application.…
The throttling refrigeration system for high cooling power recovery of the PandaX-xT cryogenic distillation system for radon removal
SJTU Paris Elite Institute of Technology, Shanghai Jiao Tong University（上海交通大学巴黎卓越工程师学院）；New Cornerstone Science Laboratory, Tsung-Dao Lee Institute, Shanghai Jiao Tong University（新Cornerstone科学实验室，汤川秀树研究所，上海交通大学）；School of Physics and Astronomy, Shanghai Jiao Tong University（上海交通大学物理与天文学院）；Shanghai Jiao Tong University Sichuan Research Institute（上海交通大学四川研究院）；Jinping Deep Underground Frontier Science and Dark Matter Key Laboratory of Sichuan Province（四川省锦屏深地下前沿科学与暗物质重点实验室）；Vacree Technologies Co., Ltd.（沃瑞科技有限公司）；School of Chemical Engineering, Zhengzhou University（郑州大学化学工程与应用学院）；School of Physics, Sun Yat-Sen University（中山大学物理学院）；Department of Physics, University of Maryland, College Park（马里兰大学帕克分校物理系）；Yalong River Hydropower Development Company, Ltd.（雅砻江流域水电开发有限公司）
In recent years cooling technology for Liquid Xenon (LXe) detectors has advanced driven by the development of Dark Matter (DM) detectors with target mass in the 100 - 1,000 kg range. The next generation of DM detectors based on LXe will be in the 50,000 kg (50 t) range requiring more than 1 kW of cooling power. Most of the prior cooling methods become impractical at this level. For cooling a 50 t scale LXe detector, a method is proposed in which Liquid Nitrogen (LN$_2$) in a small local reservoir cools the xenon gas via a cold finger. The cold finger incorporates a heating unit to provide temp…
As liquid xenon detectors grow in scale, novel techniques are required to maintain sufficient purity for charges to survive across longer drifts. The Xeclipse test facility at Columbia University was built to test the removal of electronegative impurities through cryogenic filtration powered by a liquid xenon pump, enabling a far higher mass flow rate than gas-phase purification through heated getters. In this paper, we present results from Xeclipse, including measured oxygen removal rates for two sorbent materials, which were used to guide the design and commissioning of the XENONnT liquid pu…
The radioactive isomer $^{83\mathrm{m}}$Kr has many properties that make it very useful for various applications. Its low energy decay products, like conversion, shake-off and Auger electrons as well as X- and $γ$-rays are used for calibration purposes in neutrino mass experiments and direct dark matter detection experiments. Thanks to the short half-life of 1.83 h and the decay to the ground state $^{83}$Kr, one does not risk contamination of any low-background experiment with long- lived radionuclides. In this paper, we present two new applications of $^{83\mathrm{m}}$Kr. It can be used as a…
We report a demonstration of the scalability of optically transparent xenon in the solid phase for use as a particle detector above a kilogram scale. We employ a liquid nitrogen cooled cryostat combined with a xenon purification and chiller system to measure the scintillation light output and electron drift speed from both the solid and liquid phases of xenon. Scintillation light output from sealed radioactive sources is measured by a set of high quantum efficiency photomultiplier tubes suitable for cryogenic applications. We observed a reduced amount of photons in solid phase compared to that…
The detection of scintillation light from liquid argon is an experimental technique key to a number of current and future nuclear/particle physics experiments, such as neutrino physics, neutrinoless double beta decay and dark matter searches. Although the idea of adding small quantities of xenon (doping) to enhance the light yield has attracted considerable interest, this technique has never been demonstrated at the necessary scale or precision. Here we report on xenon doping in a 100 l cryogenic vessel. Xenon doping was performed in four concentrations of 1.00$\pm$0.06 ppm, 2.0$\pm$0.1 ppm, 5…
We report the WIMP dark matter search results using the first physics-run data of the PandaX-II 500 kg liquid xenon dual-phase time-projection chamber, operating at the China JinPing Underground Laboratory. No dark matter candidate is identified above background. In combination with the data set during the commissioning run, with a total exposure of 3.3$\times10^4$ kg-day,the most stringent limit to the spin-independent interaction between the ordinary and WIMP dark matter is set for a range of dark matter mass between 3.5 and 1000 GeV/c$^2$. The best upper limit on the scattering cross sectio…
Liquid argon detectors are employed in a wide variety of nuclear and particle physics experiments. The addition of small quantities of xenon to argon modifies its scintillation, ionization, and electroluminescence properties and can improve its performance as a detection medium. However, a liquid argon-xenon mixture can develop instabilities, especially in systems that require phase transitions or that utilize high xenon concentrations. In this work, we discuss the causes for such instabilities and describe a small (liter-scale) apparatus with a unique cryogenic circuit specifically designed t…
A high-flow radon removal system based on cryogenic distillation was developed and constructed to reduce radon-induced backgrounds in liquid xenon detectors for rare event searches such as XENONnT. A continuous purification of the XENONnT liquid xenon inventory of 8.4 tonnes at process flows up to 71 kg/h (200 slpm) is required to achieve a radon reduction by a factor two for radon sources inside the detector. To reach such high flows, the distillation column's design features liquid xenon inlet and outlets along with novel custom-made bath-type heat exchangers with high liquefaction capabilit…
Silicon Photomultipliers (SiPMs) are considered as a solid-state sensor alternative to photomultiplier tubes in experiments using liquid xenon (LXe) as a radiation detection medium. The main requirements are single-photon detection of the vacuum ultraviolet scintillation light from LXe at 178$\,$nm with high resolution and detection efficiency and low noise rates. Further requirements for dark matter and double beta decay searches are ultra-low radioactivity levels of all the components including the substrates and cold electronics. Here we describe our characterisation of Hamamatsu 6$\times$6…
An important background in detectors using liquid xenon for rare event searches arises from the decays of radon and its daughters. We report for the first time a reduction of $^{222}$Rn in the gas phase above a liquid xenon reservoir. We show a reduction factor of $\gtrsim 4$ for the $^{222}$Rn concentration in boil-off xenon gas compared to the radon enriched liquid phase. A semiconductor-based $α$-detector and miniaturized proportional counters are used to detect the radon. As the radon depletion in the boil-off gas is understood as a single-stage distillation process, this result establishe…
