Cryogenic frequency-domain electron spin resonance spectrometer based on coplanar waveguides and field modulation
Björn Miksch, Martin Dressel, Marc Scheffler
备注：
The following article has been accepted by Review of Scientific Instruments. After it is published, it will be found at https://doi.org/10.1063/1.5141461
发表信息：
Review of Scientific Instruments 91, 025106 (2020)
We present an instrument to perform frequency-domain electron spin resonance (ESR) experiments that is based on coplanar waveguides and field modulation. A large parameter space in frequency (up to 25 GHz), magnetic field (up to 8 T), and temperature (down to 1.6 K) is accessible. We performed experiments on DPPH (2,2-diphenyl-1-picrylhydrazyl) as a standard to calibrate the field modulation as well as on a carbon fibre sample to estimate the overall sensitivity of the instruments. Spectra of a ruby sample in a broad frequency- and field range at cryogenic temperatures are recorded with and without field modulation. The comparison reveals the improved signal-to-noise ratio achieved by field modulation.
This paper describes a THz transmission spectrometer for the spectral range of 2-65 cm^-1 (100 GHz to 2 THz) with a spectral resolution of at least 1.8 cm^-1 (50 GHz) where the source, sample, and detector are all fully contained in a cryogenic environment. Cyclotron emission from a two-dimensional electron gas heated with an electrical current serves as a magnetic field tunable source. The spectrometer is demonstrated at 4.2 K by measuring the resonant cyclotron absorption of a second two dimensional electron gas. Unique aspects of the spectrometer are that 1) an ultra-broadband detector is u…
Development and validation of a cryogenic far-infrared diffraction grating spectrometer used to post-disperse the output from a Fourier transform spectrometer
The paper describes a radio frequency (RF) spectrometer for 14N nuclear quadrupole resonance (NQR) spectroscopy that uses a detector coil cooled to 77 K to maximize measurement sensitivity. The design uses a minimally-intrusive network of active duplexers and mechanical contact switches to realize a digitally reconfigurable series/parallel coil tuning network that allows transmit- and receive-mode performance to be independently optimized. The design is battery-powered and includes a mixed-signal embedded system to monitor and control secondary processes, thus enabling autonomous operation. Te…
The KATRIN experiment will determine the effective electron anti-neutrino mass with a sensitivity of 200 meV/c$^2$ at 90% CL. The energy analysis of tritium $β$-decay electrons will be performed by a tandem setup of electrostatic retarding spectrometers which have to be operated at very low background levels of $<10^{-2}$ counts per second. This benchmark rate can be exceeded by background processes resulting from the emanation of single $^{219,220}$Rn atoms from the inner spectrometer surface and an array of non-evaporable getter strips used as main vacuum pump. Here we report on a the impact…
The current state of far-infrared astronomy drives the need to develop compact, sensitive spectrometers for future space and ground-based instruments. Here we present details of the $\rm μ$-Spec spectrometers currently in development for the far-infrared balloon mission EXCLAIM. The spectrometers are designed to cover the $\rm 555 - 714\ μ$m range with a resolution of $\rm R\ =\ λ/ Δλ =\ 512$ at the $\rm 638\ μ$m band center. The spectrometer design incorporates a Rowland grating spectrometer implemented in a parallel plate waveguide on a low-loss single-crystal Si chip, employing Nb microstri…
We have previously used an array of cryogenic microcalorimeters with 4 eV energy resolution to measure emission-line profiles and energies of the characteristic L-shell x rays of four elements of the lanthanide series: praseodymium, neodymium, terbium, and holmium. We consider the power of the same data set for the estimation of the lines' relative intensities. Intensities must be corrected for detector efficiency and self-absorption, and we estimate uncertainties on the corrections. These data represent one of the first uses of cryogenic energy-dispersive sensors to estimate the relative inte…
We report here the realization and commissioning of an experiment dedicated to the study of the optical properties of light matter hybrids constituted of crystalline samples embedded in an optical cavity. The experimental assembly developed offers the unique opportunity to study the weak and strong coupling regime between a tunable optical cavity in cryogenic environment and low energy degrees of freedom such as phonons, magnons or charge fluctuations. We describe here the setup developed which allows the positioning of crystalline samples in an optical cavity of different quality factor, the …
We describe an instrument which can be used to analyze complex chemical mixtures at high resolution and high sensitivity. Molecules are collisionally cooled with helium gas at cryogenic temperatures (~ 4-7 K), and subsequently detected using chirped pulse microwave spectroscopy. Here we demonstrate three significant improvements to the apparatus relative to an earlier version: (1) extension of its operating range by more than a factor of two, from 12-18 GHz to 12-26 GHz, which allows a much wider range of species to be characterized; (2) improved detection sensitivity owing to use of cryogenic…
This work evaluates the viability of polyimide and parylene-C for passivation of lithium-drifted silicon (Si(Li)) detectors. The passivated Si(Li) detectors will form the particle tracker and X-ray detector of the General Antiparticle Spectrometer (GAPS) experiment, a balloon-borne experiment optimized to detect cosmic antideuterons produced in dark matter annihilations or decays. Successful passivation coatings were achieved by thermally curing polyimides, and the optimized coatings form an excellent barrier against humidity and organic contamination. The passivated Si(Li) detectors deliver $…
The ATHENA X-ray Observatory is the second large-class mission in the ESA Cosmic Vision 2015-2025 science programme. One of the two on-board instruments is the X-IFU, an imaging spectrometer based on a large array of TES microcalorimeters. To reduce the particle-induced background, the spectrometer works in combination with a Cryogenic Anticoincidence detector (CryoAC), placed less than 1 mm below the TES array. The last CryoAC single-pixel prototypes, namely AC-S7 and AC-S8, are based on large area (1 cm2) Silicon absorbers sensed by 65 parallel-connected iridium TES. This design has been ado…
The X-IFU is the cryogenic spectrometer onboard the future ATHENA X-ray observatory. It is based on a large array of TES microcalorimeters, which works in combination with a Cryogenic AntiCoincidence detector (CryoAC). This is necessary to reduce the particle background level thus enabling part of the mission science goals. Here we present the first joint test of X-IFU TES array and CryoAC Demonstration Models, performed in a FDM setup. We show that it is possible to operate properly both detectors, and we provide a preliminary demonstration of the anti-coincidence capability of the system ach…
We describe instrumentation for a high-frequency electron paramagnetic resonance (EPR) and pulsed electron-electron double resonance (PELDOR) spectroscopy. The instrumentation is operated in the frequency range of 107$-$120 GHz and 215$-$240 GHz and in the magnetic field range of 0$-$12.1 Tesla. The spectrometer consisting of a high-frequency high-power solid-state source, a quasioptical system, a phase-sensitive detection system, a cryogenic-free superconducting magnet and a $^4$He cryostat enables multi-frequency continuous-wave EPR spectroscopy as well as pulsed EPR measurements with a few …
Room Temperature Terahertz Spectrometer with Quantum-Level Sensitivity
University of California Los Angeles（加州大学洛杉矶分校）；University of Michigan, Ann Arbor（密歇根大学安娜堡分校）；Jet Propulsion Laboratory, California Institute of Technology（加州理工学院喷气推进实验室）
Advances in both instrumentation and data analysis software are now enabling the first ultra-high-resolution microcalorimeter gamma spectrometers designed for implementation in nuclear facilities and analytical laboratories. With approximately ten times better energy resolution than high-purity germanium detectors, these instruments can overcome important uncertainty limits. Microcalorimeter gamma spectroscopy is intended to provide nondestructive isotopic analysis capabilities with sufficient precision and accuracy to reduce the need for sampling, chemical separations, and mass spectrometry t…
We report on the development and demonstration of a MHz frequency domain multiplexing (FDM) technology to read out arrays of cryogenic transition edge sensor (TES) X-ray microcalorimeters. In our FDM scheme, TESs are AC-biased at different resonant frequencies in the low MHz range through an array of high-$Q$ LC resonators. The current signals of all TESs are summed at superconducting quantum interference devices (SQUIDs). We have demonstrated multiplexing for a readout of 31 pixels using room temperature electronics, high-$Q$ LC filters and TES arrays developed at SRON, and SQUID arrays from …
Athena is a space-based X-ray observatory intended for exploration of the hot and energetic universe. One of the science instruments on Athena will be the X-ray Integrated Field Unit (X-IFU), which is a cryogenic X-ray spectrometer, based on a large cryogenic imaging array of Transition Edge Sensors (TES) based microcalorimeters operating at a temperature of 100mK. The imaging array consists of 3800 pixels providing 2.5 eV spectral resolution, and covers a field of view with a diameter of of 5 arc minutes. Multiplexed readout of the cryogenic microcalorimeter array is essential to comply with …
We proposed a new high resolution single photon infrared spectrometer for search for radiative decay of cosmic neutrino background(C$ν$B). The superconducting-tunnel-junctions(STJs) are used as a single photoncounting device. Each STJ consists of Nb/Al/Al${}_{\mathrm{x}}$O${}_{\mathrm{y}}$/Al/Nb layers and their thicknesses are optimized for the operation temperature at 370 mK cooled by a ${}^{3}$He sorption refrigerator. Our STJs achieved the leak current 250 pA and the measured data implies that a smaller area STJ fulfills our requirement. FD-SOI MOSFETs are employed to amplify the STJ signa…
