arXivDaily arXiv每日学术速递 周一至周五更新
arXiv周末暂无论文更新,休息一下吧,周末愉快~~
arXiv 2008.08801cond-mat.mtrl-sci
收藏

原子探针层析成像中的优先蒸发:一种解析方法

Preferential evaporation in atom probe tomography: an analytical approach

Constantinos Hatzoglou, Solène Rouland, Bertrand Radiguet, Auriane Etienne, Gérald da Costa, Xavier Sauvage, Philippe Pareige, François Vurpillot

摘要:

原子探针层析成像(APT)分析条件在成分测量精度中起着重要作用。优先蒸发,显着偏置表观组成,比其他众所周知的现象,在APT,是密切相关的分析条件。因此,为了获得最准确的测量,优化它们的一种方法是能够预测并然后估计它们对表观组成的影响。提出了一个分析模型来量化优先蒸发。该模型适用于三种不同的合金:NiCu,FeCrNi和FeCu。该模型不仅解释了分析温度的依赖性,在现有的模型,但也依赖于脉冲分数和脉冲频率。此外,该模型还可以提供能量常数直接链接到能量势垒,需要从样品表面场蒸发原子。2

英文摘要:

Atom probe tomography (APT) analysis conditions play a major role in the composition measurement accuracy. Preferential evaporation, which significantly biases apparent composition, more than other well-known phenomena in APT, is strongly connected to those analysis conditions. One way to optimize them, in order to have the most accurate measurement, is therefore to be able to predict and then to estimate their influence on the apparent composition. An analytical model is proposed to quantify the preferential evaporation. This model is applied to three different alloys: NiCu, FeCrNi and FeCu. The model explains not only the analysis temperature dependence, as in already existing model, but also the dependence to the pulse fraction and the pulse frequency. Moreover, the model can also provide energetic constant directly linked to energy barrier, required to field evaporate atom from the sample surface. 2

机构、总结、中文摘要均由AI分析而来,可能存在错误,请以论文正文为准。

↑