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arXiv 0810.2438cond-mat.supr-concond-mat.mtrl-sci
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高能球磨和合成温度对提高MgB2非原位带材和线材超导性能的研究

High-energy ball milling and synthesi temperature study to improve superconducting properties of MgB2 ex-situ tapes and wires

Gennaro Romano, Maurizio Vignolo, Valeria Braccini, Cristina Bernini, Andrea Malagoli, Matteo Tropeano, Carlo Fanciulli, Marina Putti, Carlo Ferdeghini

摘要:

采用高能球磨法和低温合成法制备了MgB 2单组分镍包带和丝材。所有样品均在920 ℃下在Ar气流中烧结。调整研磨时间和旋转速度以使临界场电流密度(Jc)最大化:在5 K和4 T下获得6 X 10 e4 A/cm 2的最大Jc值,对应于用在180 rpm下研磨144小时的粉末制备的带。还研究了不同的合成温度(730-900 ℃),发现用在745 ℃下合成的粉末制备的线材的最佳Jc值。我们推测,这一最佳温度是由于未反应的镁含量在烧结过程之前的流化作用,可以更好地连接晶粒。

英文摘要:

MgB2 monofilamentary nickel-sheated tapes and wires were fabricated by means of the ex-situ powder-in-tube method using either high-energy ball milled and low temperature synthesized powders. All sample were sintered at 920 C in Ar flow. The milling time and the revolution speed were tuned in order to maximize the critical current density in field (Jc): the maximum Jc value of 6 x 10e4 A/cm2 at 5 K and 4 T was obtained corresponding to the tape prepared with powders milled for 144h at 180rpm. Vorious synthesis temperature were also investigated (730-900 C) finding a best Jc value for the wire prepared with powders synthesized at 745 C. We speculate that this optimal temperature is due to the fluidifying effect of unreacted magnesium content before the sintering process which could better connect the grains.

机构、总结、中文摘要均由AI分析而来,可能存在错误,请以论文正文为准。

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