We report a scanning superconducting quantum interference device (SQUID) microscope in a cryogen-free dilution refrigerator with a base temperature at the sample stage of at least 30 mK. The microscope is rigidly mounted to the mixing chamber plate to optimize thermal anchoring of the sample. The microscope housing fits into the bore of a superconducting vector magnet, and our design accommodates a large number of wires connecting the sample and sensor. Through a combination of vibration isolation in the cryostat and a rigid microscope housing, we achieve relative vibrations between the SQUID and sample that allow us to image with micrometer resolution over a 150 $μ$m range while the sample stage temperature remains at base temperature. To demonstrate the capabilities of our system, we show images acquired simultaneously of the static magnetic field, magnetic susceptibility, and magnetic fields produced by a current above a superconducting micrometer-scale device.
Temperature below 100 microKelvin is achieved in a customized cryogen-free dilution refrigerator with a copper-nuclear demagnetization stage. The lowest temperature of conduction electrons of the demagnetization stage is below 100 microKelvin as measured by a pulsed platinum NMR thermometer and the temperature can remain below 100 microKelvin for over 10 hours. An up to 9 T demagnetization magnetic field and an up to 12 T research magnetic field can be controlled independently, provided by a coaxial room-temperature-bore cryogen-free magnet.
We report on our design of a scanning gate microscope housed in a cryogen-free dilution refrigerator with a base temperature of 15 mK. The recent increase in efficiency of pulse tube cryocoolers has made cryogen-free systems popular in recent years. However, this new style of cryostat presents challenges for performing scanning probe measurements, mainly as a result of the vibrations introduced by the cryocooler. We demonstrate scanning with root-mean-square vibrations of 0.8 nm at 3 K and 2.1 nm at 15 mK in a 1 kHz bandwidth with our design.
We present a microwave quantum refrigeration principle based on the Josephson effect. When a superconducting quantum interference device (SQUID) is pierced by a time-dependent magnetic flux, it induces changes in the macroscopic quantum phase and an effective finite bias voltage appears across the SQUID. This voltage can be used to actively cool well below the lattice temperature one of the superconducting electrodes forming the interferometer. The achievable cooling performance combined with the simplicity and scalability intrinsic to the structure pave the way to a number of applications in …
Cryogen-free low-temperature setups are becoming more prominent in experimental science due to their convenience and reliability, and concern about the increasing scarcity of helium as a natural resource. Despite not having any moving parts at the cold end, pulse tube cryocoolers introduce vibrations that can be detrimental to the experiments. We characterize the coupling of these vibrations to the electrical signal observed on cables installed in a cryogen-free dilution refrigerator. The dominant electrical noise is in the 5 to 10 kHz range and its magnitude is found to be strongly temperatur…
We present a parallel network of 16 demagnetization refrigerators mounted on a cryofree dilution refrigerator aimed to cool nanoelectronic devices to sub-millikelvin temperatures. To measure the refrigerator temperature, the thermal motion of electrons in a Ag wire -- thermalized by a spot-weld to one of the Cu nuclear refrigerators -- is inductively picked-up by a superconducting gradiometer and amplified by a SQUID mounted at 4 K. The noise thermometer as well as other thermometers are used to characterize the performance of the system, finding magnetic field independent heat-leaks of a few …
We present the design and implementation of a mechanical low-pass filter vibration isolation used to reduce the vibrational noise in a cryogen-free dilution refrigerator operated at 10 mK, intended for scanning probe techniques. We discuss the design guidelines necessary to meet the competing requirements of having a low mechanical stiffness in combination with a high thermal conductance. We demonstrate the effectiveness of our approach by measuring the vibrational noise levels of an ultrasoft mechanical resonator positioned above a SQUID. Starting from a cryostat base temperature of 8 mK, the…
We have developed a system for tapered fiber measurements of optomechanical resonators inside a dilution refrigerator, which is compatible with both on- and off-chip devices. Our apparatus features full three-dimensional control of the taper-resonator coupling conditions enabling critical coupling, with an overall fiber transmission efficiency of up to 70%. Notably, our design incorporates an optical microscope system consisting of a coherent bundle of 37,000 optical fibers for real-time imaging of the experiment at a resolution of $\sim$1 $μ$m. We present cryogenic optical and optomechanical …
We present the design and operation of a fiber-based cryogenic confocal microscope. It is designed as a compact cold-finger that fits inside the bore of a superconducting magnet, and which is a modular unit that can be easily swapped between use in a dilution refrigerator and other cryostats. We aimed at application in quantum optical experiments with electron spins in semiconductors and the design has been optimized for driving with, and detection of optical fields with well-defined polarizations. This was implemented with optical access via a polarization maintaining fiber together with Voig…
Highly-Linear Proximity-Based Bi-SQUID Operating above 4 K
NEST, Istituto Nanoscienze-CNR and Scuola Normale Superiore（意大利国家纳米科学研究所与比萨高等师范学院）；INFN Sezione di Pisa（意大利国家核物理研究所比萨分部）；Quantum and Nano Technology Group, School of Chemical Engineering, The University of Adelaide（阿德莱德大学化学工程学院量子与纳米技术小组）
Magnetic fields are a standard tool in the toolbox of every physicist, and are required for the characterization of materials, as well as the polarization of spins in nuclear magnetic resonance or electron paramagnetic resonance experiments. Quite often a static magnetic field of sufficiently large, but fixed magnitude is suitable for these tasks. Here we present a permanent magnet assembly that can achieve magnetic field strengths of up to 1.5T over an air gap length of 7mm. The assembly is based on a Halbach array of neodymium (NdFeB) magnets, with the inclusion of the soft magnetic material…
A superconducting flux qubit is inductively coupled to a Superconducting QUantum Interference Device (SQUID) magnetometer, capacitively shunted to form a 1.294-GHz resonator. The qubit-state-dependent resonator frequency is weakly probed with a microwave signal and detected with a Microstrip SQUID Amplifier. At a mean resonator occupation $\bar{n}$ = 1.5 photons, the readout visibility is increased by a factor of 4.5 over that using a cryogenic semiconductor amplifier. As $\bar{n}$ is increased from 0.008 to 0.1, no reduction in $T_1$ is observed, potentially enabling continuous monitoring of …
We describe the design, construction, and performance of an ultra-high vacuum (UHV) scanning tunneling microscope (STM) capable of imaging at dilution-refrigerator temperatures and equipped with a vector magnet. The primary objective of our design is to achieve a high level of modularity by partitioning the STM system into a set of easily separable, interchangeable components. This naturally segregates the UHV needs of STM instrumentation from the typically non-UHV construction of a dilution refrigerator, facilitating the usage of non-UHV materials while maintaining a fully bakeable UHV chambe…
We present a combined scanning force and tunneling microscope working in a dilution refrigerator that is optimized for the study of individual electronic nano-devices. This apparatus is equipped with commercial piezo-electric positioners enabling the displacement of a sample below the probe over several hundred microns at very low temperature, without excessive heating. Atomic force microscopy based on a tuning fork resonator probe is used for cryogenic precise alignment of the tip with an individual device. We demonstrate the local tunneling spectroscopy of a hybrid Josephson junction as a fu…
