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arXiv 2009.07930physics.app-ph
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定向能量沉积增材制造的相关同步辐射X射线成像和衍射

Correlative Synchrotron X-ray Imaging and Diffraction of Directed Energy Deposition Additive Manufacturing

Yunhui Chen, Samuel J. Clark, David M. Collins, Sebastian Marussi, Simon A. Hunt, Danielle M. Fenech, Thomas Connolley, Robert C. Atwood, Oxana V. Magdysyuk, Ga… 展开作者

Yunhui Chen, Samuel J. Clark, David M. Collins, Sebastian Marussi, Simon A. Hunt, Danielle M. Fenech, Thomas Connolley, Robert C. Atwood, Oxana V. Magdysyuk, Gavin J. Baxter, Martyn A. Jones, Chu Lun Alex Leung, Peter D. Lee

摘要:

通过对镍基高温合金IN 718的原位和操作同步加速器X射线成像和衍射研究,揭示了定向能量沉积增材制造(DED-AM)的主导机理行为。使用一个独特的过程复制器,实空间相衬成像,使量化的凝固过程中的熔池边界和流动动力学。这种成像知识告知精确的衍射测量的时间分辨的微观结构相在转换和应力发展的空间分辨率为100 $μ$ m。衍射量化的热梯度,使枝晶凝固微观结构被预测和耦合的应力取向和大小。快速的冷却速率完全抑制了第二相的形成或固态再结晶。在凝固时,应力在冷却期间迅速增加到屈服强度。这一认识,结合IN 718 $'$的大凝固范围,表明累积的塑性耗尽了合金$'$的延展性,导致液化开裂。这项研究揭示了额外的基本机制,在DED-AM高度非平衡微结构的形成。

英文摘要:

The governing mechanistic behaviour of Directed Energy Deposition Additive Manufacturing (DED-AM) is revealed by a combined in situ and operando synchrotron X-ray imaging and diffraction study of a nickel-base superalloy, IN718. Using a unique process replicator, real-space phase-contrast imaging enables quantification of the melt-pool boundary and flow dynamics during solidification. This imaging knowledge informed precise diffraction measurements of temporally resolved microstructural phases during transformation and stress development with a spatial resolution of 100 $μ$m. The diffraction quantified thermal gradient enabled a dendritic solidification microstructure to be predicted and coupled to the stress orientation and magnitude. The fast cooling rate entirely suppressed the formation of secondary phases or recrystallisation in the solid-state. Upon solidification, the stresses rapidly increase to the yield strength during cooling. This insight, combined with IN718 $'$s large solidification range suggests that the accumulated plasticity exhausts the alloy$'$s ductility, causing liquation cracking. This study has revealed additional fundamental mechanisms governing the formation of highly non-equilibrium microstructures during DED-AM.

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