Anisotropy is an intrinsic factor that dictates the magnetic properties of YBCO, thus with great impact for many applications. Artificial pinning centres are often introduced in an attempt to mitigate its effect, resulting in less anisotropic electrical and magnetic properties. However, the nanoengineering of the superconductor makes the quantification of the anisotropy itself uncertain: the intrinsic anisotropy due to the layered structure, quantified by the anisotropy factor $γ$, mixes up with the additional anisotropy due to pinning. As a consequence, there is no consensus on the experimental anisotropy factor $γ$ that can result in YBCO when directional (twin planes, nanorods) or isotropic defects are present. We present here measurements of the magnetic field and angular dependent surface impedance in very different nanostructured YBCO films, grown by chemical route and by pulsed laser deposition, with different kind of defects (nanorods, twin planes, nanoparticles). We show that the surface impedance measurements are able to disentangle the intrinsic anisotropy from the directional pinning anisotropy, thanks to the possibility to extract the true anisotropic flux--flow resistivity and by correctly exploiting the angular scaling. We find in all films that the intrinsic anisotropy $γ= 5.3\pm0.7$. By contrast, the pinning anisotropy determines a much complex, feature--rich and nonuniversal, sample--dependent angular landscape.
We investigated the pinning of flux lines in a superconducting film by a regular array of magnetic antidots. The sample consists of a Co/Pt multilayer with perpendicular magnetic anisotropy in which a regular pattern of submicron holes is introduced and which is covered by a type-II superconducting Pb film. The resulting ferromagnetic/superconducting heterostructure shows a pronounced asymmetric magnetization curve with respect to the field polarity. This asymmetry clearly demonstrates that the magnetic contribution dominates the pinning potential imposed by the magnetic antidots on the superc…
We have prepared Na-doped YBa2Cu3Oy (YBa1.9Na0.1Cu3Oy +40mol%Y211) (YBNCO) and Na-free YBa2Cu3Oy (YBCO) samples by the Melt-Textured Growth (MTG) method to study the effect of doped Na ion on flux pinning. The ac susceptibility curves (acs) as well as the hysteresis loops were measured for the samples. Then the effective pinning energy (U(T,Hdc,J)), irreversibility line (Hirr(T)) and critical current density (jc(Hdc)) were determined, where T, Hdc and J are temperature, dc magnetic field and current density, respectively. We found that, with Na doping, the Hirr(T) line shifted to lower tempera…
We present the transport studies of field variation of the pinning force for the flux motion across the twin boundaries in YBaCuO single crystals. It is found that the depinning current J_c decreases with an increase in the magnetic field due to reduction of the portion of vortex lines trapped by the TB's. However, at transport currents J << J_c, the vortex velocity weakly decreases with the increased field, i.e. it is determined mainly by the release of the vortex lines from the TB's.
The transverse (Hall) voltage in thin films of the high-temperature superconductor YBa$_{2}$Cu$_{3}$O$_{7-δ}$ with an artificial periodic pinning array is investigated. Columnar defect regions along the crystallographic $c$ axis, in which superconductivity is suppressed, are created by irradiation with He$^+$ ions through a silicon stencil mask. The commensurate arrangement of magnetic flux quanta with the artificial defect lattice is confirmed by maxima of the critical current and minima of the resistance, respectively. The magnetic field dependence of the transverse voltage reveals a commens…
Measurements of the Hall effect and the resistivity in twinned YBa2Cu3O7-delta thin films in magnetic fields B oriented parallel to the crystallographic c-axis and to the twin boundaries reveal a double sign reversal of the Hall coefficient for B below 1 T. In high transport current densities, or with B tilted off the twin boundaries by 5 degrees, the second sign reversal vanishes. The power-law scaling of the Hall conductivity to the longitudinal conductivity in the mixed state is strongly modified in the regime of the second sign reversal. Our observations are interpreted as strong, disorder…
We report measurements of the irreversible magnetization M_i of a large number of YBa_2Cu_3O_7 single crystals with columnar defects (CD). Some of them exhibit a maximum in M_i when the density of vortices equals the density of tracks, at temperatures above 40K. We show that the observation of these matching field effects is constrained to those crystals where the orientational and pinning energy dispersion of the CD system lies below a certain threshold. The amount of such dispersion is determined by the mass and energy of the irradiation ions, and by the crystal thickness. Time relaxation me…
Driven vortex lattices have been studied in a material with strong pinning, such as Nb films. Samples in which natural random pinning coexists with artificial ordered arrays of defects (submicrometric Ni dots) have been fabricated with different geometries (square, triangular and rectangular). Three different dynamic regimes are found: for low vortex velocities, there is a plastic regime in which random defects frustrate the effect of the ordered array; then, for vortex velocities in the range 1-100 m/s, there is a sudden increase in the interaction between the vortex lattice and the ordered d…
The linear dynamic response of the two-dimensional (2D) vortex medium in ultrathin YBa_2Cu_3O_7 films was studied by measuring their ac sheet impedance Z over a broad range of frequencies ω. With decreasing temperature the dissipative component of Z exhibits, at a temperature T*(ω) well above the melting temperature of a 2D vortex crystal, a crossover from a thermally activated regime involving single vortices to a regime where the response has features consistent with a description in terms of a collectively pinned vortex manifold. This suggests the idea of a vortex liquid which, below T*(ω),…
The influence of low-level Pr substitution in Y1-xPrxBa2Cu3O(7-delta) single crystals on the anisotropy of the superconducting state parameters was investigated by torque magnetometry in magnetic fields of up to 9 T. An averaged anisotropy parameter, γ, of 7.4 was found and no influence of the Pr ion concentration on γwas observed up to a Pr content of 2.4%. A pronounced maximum at angles between 0.5 and 1 degree out of the ab-plane was observed in all crystals in the irreversible angular dependence of the torque. This maximum is attributed to intrinsic pinning associated with kinked vortices.…
The angular dependence of magnetic-field commensurability effects in thin films of the cuprate high-critical-temperature superconductor YBa$_{2}$Cu$_{3}$O$_{7-δ}$ (YBCO) with an artificial pinning landscape is investigated. Columns of point defects are fabricated by two different methods of ion irradiation -- scanning the focused 30 keV ion beam in a helium ion microscope or employing the wide-field 75 keV He$^+$ beam of an ion implanter through a stencil mask. Simulations of the ion-target interactions and the resulting collision cascades reveal that with both methods square arrays of defect …
Combined action of weak and strong pinning centers on the vortex lattice complicates magnetic behavior of a superconductor since temperature and magnetic field differently affect weak and strong pinning. In this paper we show that contributions of weak and strong pinning into magnetization of the layered superconductor YBa$_2$Cu$_3$O$_{7-δ}$ can be separated and analyzed individually. We performed a careful analysis of temperature behavior of the relaxed superconducting current $J$ in YBa$_2$Cu$_3$O$_{7-δ}$ films which revealed two components of the current $J = J_1 +J_2$. A simple method of s…
We present a microwave study of the angular dependence of the flux-flow resistivity $ρ_{ff}$ and of the pinning constant $k_p$ in YBCO thin films containing BZO nanorods. We find that BZO nanorods are very efficient pinning centers, even in tilted fields. We find that $ρ_{ff}$ is a scaling function of a reduced field $H/f(θ)$. We extend a model for the anisotropic motion of vortices in uniaxially anisotropic superconductor, able to describe the experimental $f(θ)$ on the basis of only the intrinsic anisotropy of YBCO. The pinning constant $k_p$, by contrast, exhibits different field dependence…
Measurements of anisotropic transport properties (dc and high-frequency regime) of driven vortex matter in YBa$_2$Cu$_3$O$_{7-x}$ with elongated strong-pinning sites (c-axis aligned, self-assembled BaZrO$_3$ nanorods) are used to demonstrate that the effective-mass angular scaling takes place only in intrinsic physical quantities (flux-flow resistivity), and not in pinning-related Labusch parameter and critical currents. Comparison of the dynamics at different time scales shows evidence for a transition of the vortex matter toward a Mott phase, driven by the presence of nanorods. The strong pi…
By using a highly sensitive homemade AC magnetic susceptibility technique, the magnetic flux penetration has been measured in YBa_2Cu_3O_7 single crystals with giant screw dislocations (having the structure of the Archimedean spirals) exhibiting a=3 spiral turnings, the pitch b=18.7 microns and the step height c=1.2nm (the last parameter is responsible for creation of extended weak-link structure around the giant defects). The magnetic field applied parallel to the surface enters winding around the weak-link regions of the screw in the form of the so-called spiral Josephson fluxons characteriz…
We investigate the effect of the anisotropy and of the directional pinning in YBa$_2$Cu$_3$O$_{7-x}$ films grown by pulsed laser ablation from targets containing BaZrO$_3$ at 5% mol. BaZrO$_3$ inclusions self-assemble to give nanorods oriented along the c-axis, thus giving a preferential direction for vortex pinning. The directionality of vortex response is studied at high ac frequency with the complex microwave response at 48 GHz, as a function of the applied field and of the angle $θ$ between the field and the c-axis. The complex microwave response does not exhibit any angular scaling, sugge…
The pinning properties of type-II superconductors can be efficiently controlled by using laterally nanostructured ferromagnet / superconductor bilayers. This will be illustrated by studying the flux pinning in thin superconducting Pb films which are deposited on top of two types of magnetic nanostructures with out-of-plane magnetisation: (i) an array of dots, and (ii) an array of antidots, both made from a Co/Pt multilayer. The magnetisation curves of the Pb film are extremely asymmetric with respect to the polarity of the magnetic field when the magnetic moments in the Co/Pt multilayer were a…
Superconducting critical currents $j_{c} > 10^{5}$ A/cm$^{2}$ at temperatures $T \sim 50$ K and magnetic fields $B \sim 6$ T are reported for the YBa$_{2}$Cu$_{3-x}$Mo$_{x}$O$_{7+d}$ compound with $x = 0.02$. Clear evidence for the increased pinning force $F_p$ was found from a peak effect present for $j_{c}(B)$. The pinning force was analyzed by a scaling procedure using Kramer's approach. For a wide range of fields and temperatures, we were able to express all $F_p$ data as a single function of a reduced field $b = B/B_k$, where the scaling field $B_{k} << H_{c2}$ was related to the irrevers…
We present a study of the anisotropic vortex parameters as obtained from measurements of the microwave complex resistivity in the vortex state with a tilted applied magnetic field in YBa2Cu3O7-x thin films with BaZrO3 nanorods. We present the angular dependence of the vortex viscosity $η$, the pinning constant k_p and the upper limit for the creep factor χ_M. We show that the directional effect of the nanorods is absent in η, which is dictated by the mass anisotropy γ. By contrast, pinning-mediated properties are strongly affected by the nanorods. It is significant that the pinning and creep a…
We study the general problem of a manifold of interacting elastic lines whose spatial correlations are strongly affected by the competition between random and ordered pinning. This is done through magneto-transport experiments with YBa2Cu3O7-d thin films that contain a periodic vortex pinning array created via masked ion irradiation, in addition to the native random pinning. The strong field-matching effects we observe suggest the prevalence of periodic pinning, and indicate that at the matching field each vortex line is bound to an artificial pinning site. However, the vortex-glass transition…
In 1976 Larkin and Ovchinnikov [Sov. Phys. JETP 41, 960 (1976)] predicted that vortex matter in superconductors driven by an electrical current can undergo an abrupt dynamic transition from a flux-flow regime to a more dissipative state at sufficiently high vortex velocities. Typically this transition manifests itself as a large voltage jump at a particular current density, so-called instability current density $J^*$, which is smaller than the depairing current. By tuning the effective pinning strength in Al films, using an artificial periodic pinning array of triangular holes, we show that a …
We report complex impedance measurements in an untwinned YBaCuO crystal. Our broad frequency range covers both the quasi static response and the resistive response of the vortex lattice. It allow us to characterize the irreversibility line without the need of any frequency dependent pinning parameters. We confirm the validity of the two modes model of vortex dynamic, and extract both the surface critical current and the flux flow resistivity around the first order transition $T_{m}$. This latter is identified by the abrupt loss of pinning and by an unexpected step of $ρ_{ff}(T)$ at $T_{m}$.
There are numerous potential applications for superconducting tapes, based on YBa2Cu3O7-x (YBCO) films coated onto metallic substrates. A long established goal of more than 15 years has been to understand the magnetic flux pinning mechanisms which allow films to maintain high current densities out to high magnetic fields. In fact, films carry 1-2 orders of magnitude higher current densities than any other form of the material. For this reason, the idea of further improving pinning has received little attention. Now that commercialisation of conductors is much closer, for both better performanc…
We created local pinning modulations in YBCO films by means of confined high energy heavy ion irradiation. The high energy of the ions allows us to introduce nanometric size defects with a well defined anisotropy. The dose was chosen in such a way to reduce the local critical current of the irradiated area. We used a quantitative magneto-optical analysis to measure the magnetic field vector and the supercurrent for each point of the whole sample surface. The basic geometry of a rectangular region inside strip-shaped samples was considered in order to investigate in detail the effect of the ori…
Nano-scaled substrate surface roughness is shown to strongly influence the critical current density Jc in YBCO films made by pulse-laser-deposition on the crystalline LaAlO3 substrates consisting of two separate twin-free and twin-rich regions. The nano-scaled corrugated surface was created in the twin-rich region during the deposition process. Using magneto-optical imaging techniques coupled with optical and atomic force microscopy, we observed an enhanced flux pinning in the YBCO films in the twin-rich region, resulted in \~30% increase in Jc, which was unambiguously confirmed by the direct …
Infrared spectroscopy has been used to investigate the temperature dependence and c-axis magnetic field dependence of the Josephson plasma resonance in optimally doped Tl2Ba2CaCu2O8 thin films, and underdoped YBa2Cu3O6.5 ortho - II single crystals. The resonances are directly related to the c-axis penetration depths, yielding low temperature, zero fields values of about 20 micrometer, and 7 micrometer respectively. While the temperature dependencies of the resonances in the two compounds are very similar, the magnetic field dependence in YBCO is much weaker. We attribute this weak magnetic fie…
We have measured an angle-dependent contribution to the equilibrium magnetization of a YBa_2Cu_3O_{7-d} single crystal with columnar defects created by 5.8GeV Pb ions. This contribution manifests itself as a jump in the equilibrium torque signal, when the magnetic field crosses that of the defects. The magnitude of the signal, which is observed in a narrow temperature interval less than 2K and for fields up to about twice the irradiation field, is used to estimate the the energy gained by vortex pinning on the defects. The vanishing of the effective pinning energy at a temperature below Tc is …
We propose a simple nanostructured pinning array geometry where a rich variety of complex vortex shear banding phenomena can be realized. A single row of pinning sites is removed from a square pinning array. Shear banding effects arise when vortex motion in the pin-free channel nucleates motion of vortices in the surrounding pinned regions, creating discrete steps in the vortex velocity profile away from the channel. Near the global depinning transition, the width of the band of moving vortices undergoes oscillations or fluctuations that can span the entire system. We use simulations to show t…
Magnetic fields penetrate a type-II superconductor as magnetic flux quanta, called vortices. In a clean superconductor they arrange in a hexagonal lattice, while by adding periodic artificial pinning centers many other arrangements can be realized. Using the focused beam of a helium ion microscope we have fabricated periodic patterns of dense pinning centers with spacings as small as 70 nm in thin films of the cuprate superconductor YBa$_{2}$Cu$_{3}$O$_{7-δ}$. In these ultradense kagomé-like patterns, the voids lead to magnetic caging of vortices, resulting in unconventional commensurability e…
The ability of high-temperature superconductors (HTSs) to carry very large currents with almost no dissipation makes them irreplaceable for high-power applications. The development and further improvement of HTS-based cables requires an in-depth understanding of the superconducting vortex dynamics in presence of complex pinning landscapes. We present a critical current analysis of a real HTS sample in a magnetic field by combining state-of-the-art large-scale Ginzburg-Landau simulations with reconstructive three-dimensional scanning transmission electron microscopy tomography of the pinning la…
An advanced mask-less nanofabrication technique, focused electron beam-induced deposition (FEBID), has been employed on epitaxial Nb thin films for their ferromagnetic decoration by an array of Co stripes. These substantially modify the non-patterned films' superconducting properties, providing a washboard-like pinning potential landscape for the vortex motion. At small magnetic fields B<0.1T, vortex lattice matching effects have been investigated by magneto-transport measurements. Peculiarities in the field dependencies of the films resistivity R(B) have been observed in particular for the vo…
We probe the short-range pinning properties with the application of microwave currents at very high driving frequencies (47.7 GHz) on YBa$_2$Cu$_3$O$_{7-δ}$ films with and without sub-micrometer BaZrO$_3$ inclusions. We explore the temperature and field ranges 60 K$<T<T_c$ and 0$<μ_0H<$0.8 T, with the field applied along the c-axis. The magnetic field induces a much smaller increase of the microwave resistivity, $Δρ_1(H)+\mathrm{i}Δρ_2(H)$, in YBa$_2$Cu$_3$O$_{7-δ}$/BaZrO$_3$ with respect to pure YBa$_2$Cu$_3$O$_{7-δ}$. $Δρ_1(H)$ is slightly superlinear in pure YBa$_2$Cu$_3$O$_{7-δ}$ (suggesti…
The design of artificial vortex pinning landscapes is a major goal towards large scale applications of cuprate superconductors. While disordered nanometric inclusions have shown to modify their vortex phase diagram and to produce enhancements of the critical current1,2, the effect of ordered oxide nanostructures remains essentially unexplored. This is due to the very small nanostructure size imposed by the short coherence length, and to the technological difficulties in the nanofabrication process. Yet, the novel phenomena occurring at oxide interfaces open a wide spectrum of technological opp…
It is shown that the large effect of heavy ion-irradiation on the thermodynamical properties of the anisotropic superconductor YBa$_{2}$Cu$_{3}$O$_{7-δ}$ extends well into the superconducting fluctuation regime. The presence of the induced amorphous columnar defects shifts the specific heat maximum at the normal-to-superconducting transition. This effect is similar to that recently put into evidence in cubic K$_{x}$Ba$_{1-x}$BiO$_{3}$ ($x \simeq 0.35$). In both compounds, vortex pinning manifests itself as a sharp angular dependence of the \em equilibrium \rm torque. In YBa$_{2}$Cu$_{3}$O$_{7-…
The competition between intrinsic disorder in superconducting YBa$_{2}$Cu$_{3}$O$_{7-δ}$ (YBCO) thin films and an ultradense triangular lattice of cylindrical pinning centers spaced at 30 nm intervals results in an ordered Bose glass phase of vortices. The samples were created by scanning the focused beam of a helium-ion microscope over the surface of the YBCO thin film to form columns of point defects where superconductivity was locally suppressed. The voltage-current isotherms reveal critical behavior and scale in the vicinity of the second-order glass transition. The latter exhibits a disti…
In this paper we present our results on the low density magnetic flux pinning characteristics, obtained though HTSC samples magnetization relaxation measurements M(t) near the phase transition temperatures (0,8 < T/Tc > 0,99).As the main object of investigation we have chosen pure YBa2Cu3O7-x (YBCO) single crystal samples with optimal oxygen saturation. We note the presence of strong pinning in the system of unidirectional planar defects and a significant nonmonotonicity of the Up(T) dependence behavior for low density trapped magnetic flux.
We present measurements of the microwave complex surface impedance at 47.7 GHz in YBa$_2$Cu$_3$O$_{7-δ}$ (YBCO) films deposited by pulsed laser deposition with the explicit goal to introduce BaZrO$_3$ (BZO) nanoinclusions. Composite targets obtained by addition of BZO powder in molar percents ranging from 2.5 to 7 mol.% have been prepared and characterized. Measurements of the microwave surface impedance indicate a broadened transition in zero field, however compensated by a very large pinning frequency, indicating that while intergrain properties are still to be optimized the effect of nanome…
We present a new experiment on YBa_2Cu_3O_{7-x} (YBCO) thin films using spatially resolved heavy ion irradiation. Structures consisting of a periodic array of strong and weak pinning channels were created with the help of metal masks. The channels formed an angle of +/-45 Deg with respect to the symmetry axis of the photolithographically patterned structures. Investigations of the anisotropic transport properties of these structures were performed. We found striking resemblance to guided vortex motion as it was observed in YBCO single crystals containing an array of unidirected twin boundaries…
In order to study the vortex pinning determined by artificially introduced pinning centers in the small-vortex displacement regime, we measured the microwave surface impedance at 47.7 GHz in the mixed state of YBa$_{2}$Cu$_{3}$O$_{7-δ}$ thin films, where sub-micrometric BaZrO$_3$ particles have been incorporated. As a function of the BaZrO$_3$ content, we observe that the absolute losses slightly decrease up to a BaZrO$_3$ content of 5%, and then increase. We found that the magnetic-field-induced losses behave differently, in that they are not monotonic with increasing BaZrO$_3$ concentration:…
The effect of the transverse AC magnetic field on relaxation process in YBa$_2$Cu$_3$O$_x$ melt-textured superconductor was studied. A factor of 50 suppression of the relaxation rate could be achieved at the expense of some reduction in the maximum trapped field, with the magnetic-induction gradient being unchanged. This phenomenon is interpreted as a result of an increase of the pinning force after the action of the transverse AC magnetic field that is confirmed by the measurement of the trapped-induction distribution.
We analyze the angular dependence of the irreversible magnetization of YBa$_2$Cu$_3$O$_7$ crystals with columnar defects inclined from the c-axis. At high fields a sharp maximum centered at the tracks' direction is observed. At low fields we identify a lock-in phase characterized by an angle-independent pinning strength and observe an angular shift of the peak towards the c-axis that originates in the material anisotropy. The interplay among columnar defects, twins and ab-planes generates a variety of staircase structures. We show that correlated pinning dominates for all field orientations.
We observe a strong reduction of the field induced thin film surface resistance measured at high microwave frequency ($ν=$47.7 GHz) in YBa$_{2}$Cu$_{3}$O$_{7-δ}$ thin films grown on SrTiO$_3$ substrates, as a consequence of the introduction of sub-micrometric BaZrO$_3$ particles. The field increase of the surface resistance is smaller by a factor of $\sim$3 in the film with BaZrO$_3$ inclusions, while the zero-field properties are not much affected. Combining surface resistance and surface reactance data we conclude (a) that BaZrO$_3$ inclusions determine very deep and steep pinning wells and …
We report on measurements on Y1-xPrxBa2Cu3O7-delta single crystals, with x varying from 0 to 2.4%. The upper and the lower critical fields, Hc2 and Hc1, the Ginzburg-Landau parameter and the critical current density, Jc(B), were determined from magnetization measurements and the effective media approach scaling method. We present the influence of Pr substitution on the pinning force density as well as on the trapped field profiles analyzed by Hall probe scanning.
We use magnetic force microscopy to both image and manipulate individual vortex lines threading single crystalline YBa$_2$Cu$_3$O$_{6.4}$, a layered superconductor. We find that when we pull the top of a pinned vortex, it may not tilt smoothly. Sometimes, we observe a vortex to break into discrete segments that can be described as short stacks of pancake vortices, similar to the "kinked" structure proposed by Benkraouda and Clem. Quantitative analysis gives an estimate of the pinning force and the coupling between the stacks. Our measurements highlight the discrete nature of stacks of pancake …
In order to compare magnetic and non-magnetic pinning we have nanostructured two superconducting films with regular arrays of pinning centers: Cu (non-magnetic) dots in one case, and Py (magnetic) dots in the other. For low applied magnetic fields, when all the vortices are pinned in the artificial inclusions, magnetic dots prove to be better pinning centers, as has been generally accepted. Unexpectedly, when the magnetic field is increased and interstitial vortices appear, the results are very different: we show how the stray field generated by the magnetic dots can produce an effective reduc…
$M(B)$-curves were experimentally investigated. Fishtail-effect (FE) was observed in MG YBa$_2$Cu$_3$O$_{7-δ}$ and YBa$_2$(Cu$_{1-x}$Ag$_x$)$_3$O$_{7-δ}$ (at $x \approx$ 0.02) crystals in a wide temperature range 0.4 $<T/T_c<$ 0.8 at the orientation of magnetic field $\textbf{H}\parallel c$. It was obtained that the influence of bulk pinning on FE is more effective at low temperatures while surface barriers dominates at high temperatures. The value $H_{max}$ for Ag-doped crystals is larger than for a pure one that due to the presence of additional pinning centers, above all on silver atoms.
$M(B)$-curves were experimentally investigated. Fishtail-effect (FE) was observed in MG YBa$_2$Cu$_3$O$_{7-δ}$ and YBa$_2$Cu$_{3-x}$Ag$_x$O$_{7-δ}$ (at $x \approx$ 0.02) crystals in a wide temperature range 40 K $<T<$ 75 K at the orientation of magnetic field $\textbf{H}\parallel c$. It was obtained that the influence of bulk pinning on FE is more effective at low temperatures while the influence of surface barriers is more effective at high temperatures. The value $H_{max}$ for Ag-doped crystals is larger than for a pure one that due to the presence of additional pinning centers, above all on…
We report on the field dependence of the microwave complex resistivity data in YBa$_2$Cu$_3$O$_{7-x}$/BaZrO$_3$ films grown by PLD at various BaZrO$_3$ content. The data, analyzed within a recently developed general framework for the mixed-state microwave response of superconductors, yield the field dependence of the fluxon parameters such as the vortex viscosity and the pinning constant. We find that pinning undergoes a change of regime when the BaZrO$_3$ content in the target increases from 2.5 mol.% to 5 mol.%. Simultaneously, the vortex viscosity becomes an increasing function of the appli…
We report on magnetic measurements carried out in a textured YBa$_2$Cu$_3$O$_{7-δ}$ and YBa$_2$(Cu$_{1-x}$Ag$_x$)$_3$O$_{7-δ}$ (at $x \approx$ 0.02) crystals. The so-called fishtail-effect (FE) or second magnetization peak has been observed in a wide temperature range 0.4~$<T/T_c<$~0.8 for $\textbf{H}\parallel c$. The origin of the FE arises for the competition between surface barrier and bulk pinning. This is confirmed in a non-monotonically behavior of the relaxation rate $R$. The value $H_{max}$ for Ag-doped crystals is larger than for the pure one due to the presence of additional pinning …
We present a comparative study of the angular dependent critical current density in YBa2Cu3O7 films deposited on IBAD MgO and on single crystal MgO and SrTiO3 substrates. We identify three angular regimes where pinning is dominated by different types of correlated and uncorrelated defects. We show that those regimes are present in all cases, indicating that the pinning mechanisms are the same, but their extension and characteristics are sample dependent, reflecting the quantitative differences in texture and defect density. In particular, the more defective nature of the films on IBAD turns in…
The influence of Ca substitution on the superconducting properties of polycrystalline R1-xCaxBa2Cu3Oz (R = Eu, Gd, Er; x=0; 0.2; 0.25 and 0.3) samples has been studied by X-ray powder diffraction, ac susceptibility and dc magnetization measurements. The superconducting parameters such as critical temperature, inter- and intra-granular critical current and flux pinning are found to be strongly dependent both on Ca content and type of R element. The best combination of these parameters is found for the system Gd1-xCaxBa2Cu3Oz forming R1+yBa2-yCu3Oz clusters. The level of overdoping and the type …
Demanding microwave applications in a magnetic field require the material optimization not only in zero-field but, more important, in the in-field flux motion dominated regime. However, the effect of artificial pinning centers (APC) remains unclear at high frequency. Moreover, in coated conductors the evaluation of the high frequency material properties is difficult due to the complicated electromagnetic problem of a thin superconducting film on a buffered metal substrate. In this paper we present an experimental study at 48 GHz of 150-200 nm YBa$_2$Cu$_3$O$_{7-x}$ coated conductors, with and …
We propose a phenomenological model that accounts for the history effects observed in ac susceptibility measurements in YBa2Cu3O7 single crystals [Phys. Rev. Lett. 84, 4200 (2000) and Phys. Rev. Lett. 86, 504 (2001)]. Central to the model is the assumption that the penetrating ac magnetic field modifies the vortex lattice mobility, trapping different robust dynamical states in different regions of the sample. We discuss in detail on the response of the superconductor to an ac magnetic field when the vortex lattice mobility is not uniform inside the sample. We begin with an analytical descripti…
Bulk superconductor samples of YBa2Cu3-xCoxO7-δ with x = 0, 0.01, 0.03, 0.05 are synthesized by solid-state reaction route. Both x-ray diffraction and electron microscopy have been employed to study the phase identification, intergrowths, dislocations and the local structure of these samples. Transition temperature of the samples has been determined by four probe resistivity measurements. The x-ray diffraction patterns indicate that the gross structure/ phase of YBa2Cu3-xCoxO7-δ do not change with the substitution of Co up to x=0.05. The zero resistance critical transition temperature [Tc(R=0)…
Mechanisms of vortex dynamics and pinning and self-field effects which could account for the thickness dependence of the critical current density J_c of superconducting films are addressed. It is shown that at low magnetic fields B, the 2D single-vortex pinning and thermal fluctuations yield J_c proportional to (1/sqrt{d})exp[-(d_m/d)^{1/2}], if the film thickness d is smaller than the pinning correlation length along B. The model describes the dependence of J_c on d observed on YBa_2Cu_3O_7 coated conductors for d < 2(mu)m. Measurements of J_c(d) in strong magnetic fields are proposed to prob…
In a magnetic field, superconductivity is manifested by total magnetic field expulsion (Meissner effect) or by the penetration of integer multiples of the flux quantum Φ_0. Here we present experimental results revealing magnetic dipoles formed by Meissner current flowing around artificially introduced topological defects (lattice of antidots). By using scanning Hall probe microscopy, we have detected ordered magnetic dipole lattice generated at spatially periodic antidots in a Pb superconducting film. While the conventional homogeneous Meissner state breaks down, the total magnetic flux of the…
We present measurements of the vortex-state surface impedance, Z_s = R_s + i X_s, of a high quality, ortho-II-ordered single crystal of the cuprate high temperature superconductor YBa2Cu3O6.52 (T_c = 59K). Measurements have been made at four microwave frequencies (ω/2π= 2.64, 4.51, 9.12 and 13.97 GHz), for magnetic fields ranging from 0 to 7 T. From these data we obtain the field, frequency and temperature dependence of the vortex viscosity, pinning constant, depinning frequency and flux-flow resistivity. The vortex viscosity, η(ω,T), has a surprisingly strong frequency dependence and bears a …
The superconducting phase transition in YBa$_{2}$Cu$_{3}$O$_{7-\textit{$δ$}}$(YBCO) thin film samples doped with non-superconducting nanodot impurities of CeO$_{2}$ are the focus of recent high-temperature superconductor studies. Non-superconducting holes of the superconducting lattice induce a bound-state of circulating paired electrons. This creates a magnetic flux vortex state. Examining the flow of free-electrons shows that these quantized magnetic flux vortices arrange themselves in a self-assembled lattice. The nanodots serve to present structural properties to constrict the "creep" of t…
Thin superconducting YBa$_{2}$Cu$_{3}$O$_{7-δ}$ films are patterned with a vortex-pin lattice consisting of columnar defect regions (CDs) with 180 nm diameter and 300 nm spacing. They are fabricated by irradiation with 75 keV He$^+$ ions through a stencil mask. Peaks of the critical current reveal the commensurate trapping of vortices in domains near the edges of the sample. Upon ramping an external magnetic field, the positions of the critical current peaks are shifted from their equilibrium values to lower magnetic fields in virgin and to higher fields in field-saturated down-sweep curves, r…
The critical current density of epitaxial YBCO films grown on vicinal SrTiO3 substrates was investigated by electrical transport measurements along and across the steps of the SrTiO3 surface for a range of temperatures of 10 K to 85 K and in applied magnetic fields varying from 0 to 14 T. For vicinal angles of 4 and 8 degrees, we found evidence of enhanced pinning in the longitudinal direction at low magnetic fields for a wide region of temperatures and attribute this phenomenon to anti-phase boundaries in the YBCO film. The transverse Jc data showed a peak in the Jc(H) curve at low magnetic f…
