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arXiv 2603.08968cond-mat.mtrl-sciphysics.app-ph
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利用暗场X射线显微镜对再结晶铁中晶内残余应变和微结构的3D映射

3D Mapping of Intragranular Residual Strain and Microstructure in Recrystallized Iron Using Dark-Field X-ray Microscopy

European Synchrotron Radiation Facility(欧洲同步辐射装置);Universite Lyon I, INSA Lyon, CNRS, MATEIS UMR5510(里昂第一大学、里昂国立应用科学学院、法国国家科学研究中心、MATEIS联合研究实验室)

Virginia Sanna, Yubin Zhang, Wolfgang Ludwig, Aditya Shukla, Abderrahmane Benhadjira, Marilyn Sarkis, Can Yildirim

AI总结:

本研究利用暗场X射线显微镜首次实现了对再结晶铁中晶内残余应变和微结构的三维映射,揭示了应变分布的不均匀性及位错与第二相粒子的相互作用。

摘要:

晶粒生长是金属热机械处理过程中的关键步骤。最近,完全再结晶晶粒中局部残余应力的存在引起了越来越多的关注,特别是在与剪切耦合的晶界迁移机制相关联时。在本工作中,我们提供了首次直接的实验测量结果,显示完全再结晶商用纯铁中残余弹性应变的变化,其量级约为10^-4。利用暗场X射线显微镜(DFXM),我们对单个晶粒内的应变和取向变化进行了非破坏性的三维测量。我们的结果揭示了所有测量晶粒中的应变分布不均。在一种情况下,我们观察到几条孤立的位错容纳两个第二相粒子,表现出局部应变特征,没有可检测的远距离影响。讨论了晶内残余应变的形成机制及其在随后晶粒生长过程中对晶界迁移的潜在影响。这项工作强调了在未来晶粒生长模型中考虑此类残余弹性应变的重要性。

英文摘要:

Grain growth is a key process in the thermomechanical treatment of metals. Recently, the presence of local residual stresses within fully recrystallized grains has attracted increasing interest in connection with shear-coupled grain boundary migration mechanisms. In this work, we provide the first direct experimental measurements of residual elastic strain variations in fully recrystallized commercial-purity iron, on the order of $10^{-4}$. Using dark-field X-ray microscopy (DFXM), we performed non-destructive three-dimensional measurements of strain and orientation variations within individual grains. Our results reveal heterogeneous strain distributions across all measured grains. In one case, we observed several isolated dislocations accommodating two second-phase particles, exhibiting a localized strain signature with no detectable long-range effect. The formation mechanisms of intragranular residual strains and their potential influence on grain boundary migration during subsequent grain growth are discussed. This work highlights the importance of accounting for such residual elastic strains in future grain growth models.

机构、总结、中文摘要均由AI分析而来,可能存在错误,请以论文正文为准。

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