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arXiv 2009.14512cond-mat.mtrl-scieess.IVphysics.ins-det
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快速与传统HAADF-STEM断层扫描:优势和挑战

Fast versus conventional HAADF-STEM tomography: advantages and challenges

Hans Vanrompay, Alexander Skorikov, Eva Bladt, Armand Béché, Bert Freitag, Jo Verbeeck, Sara Bals

摘要:

电子层析成像是一种广泛使用的实验技术,用于分析各种材料的三维纳米级结构。不幸的是,根据实验的复杂性,常规电子层析成像倾斜序列的采集很容易花费一个小时或更长时间。因此,使用电子断层扫描,获得统计上有意义的3D数据,调查不能承受长时间采集的样品,或使用该技术进行原位3D表征,远非简单。已经提出了各种采集策略来加速断层摄影采集,并减少所需的电子剂量。这些方法包括在获取投影电影的同时连续地倾斜保持器,以及结合了常规技术和连续技术的益处的混合、增量方法。在本文中,不同的采集策略将在速度,分辨率和电子剂量方面进行实验比较,根据实验倾斜系列获得各种金属纳米粒子。

英文摘要:

Electron tomography is a widely used experimental technique for analyzing nanometer-scale structures of a large variety of materials in three dimensions. Unfortunately, the acquisition of conventional electron tomography tilt series can easily take up one hour or more, depending on the complexity of the experiment. Using electron tomography, it is therefore far from straightforward to obtain statistically meaningful 3D data, to investigate samples that do not withstand long acquisition, or to perform in situ 3D characterization using this technique. Various acquisition strategies have been proposed to accelerate the tomographic acquisition, and reduce the required electron dose. These methods include tilting the holder continuously while acquiring a projection movie and a hybrid, incremental, methodology which combines the benefits of the conventional and continuous technique. In this paper, the different acquisition strategies will be experimentally compared in terms of speed, resolution and electron dose, based on experimental tilt series acquired for various metallic nanoparticles.

机构、总结、中文摘要均由AI分析而来,可能存在错误,请以论文正文为准。

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